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Record W4401459992 · doi:10.1021/acs.jpca.4c03890

Millimeter-Wave and High-Resolution Infrared Spectroscopy of the Ground and Seven Lowest Fundamental States of 1<i>H</i>-1,2,4-Triazole

2024· article· en· W4401459992 on OpenAlexaff
Hayley Bunn, Maria A. Zdanovskaia, Brant Billinghurst, Jianbao Zhao, Susanna L. Widicus Weaver, R. Claude Woods, Robert J. McMahon, Brian J. Esselman

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2024
Typearticle
Languageen
FieldChemistry
TopicMolecular Spectroscopy and Structure
Canadian institutionsCanadian Light Source (Canada)University of Saskatchewan
FundersDivision of Chemical, Bioengineering, Environmental, and Transport SystemsUniversity of Wisconsin-Madison
KeywordsExtremely high frequencyInfraredMillimeterInfrared spectroscopyHigh resolutionSpectroscopyResolution (logic)PhysicsMaterials scienceOpticsRemote sensingGeologyAstronomyComputer scienceQuantum mechanics

Abstract

fetched live from OpenAlex

A combined analysis of millimeter-wave (70–700 GHz) and rotationally resolved infrared (400–1200 cm –1 ) spectra of the ground state and seven fundamental vibrational modes of 1 H -1,2,4-triazole is reported. While the lowest-energy vibrationally excited state (ν 18 ) is well-treated using a single-state distorted-rotor Hamiltonian, the second (ν 17 ) and third (ν 16 ) vibrationally excited states are involved in strong c -type Coriolis coupling and require an appropriate two-state Hamiltonian. The oblate nature of 1 H -1,2,4-triazole is sufficiently close to the oblate symmetric-top limit that the analysis requires the use of A-reduced, sextic centrifugally distorted-rotor Hamiltonian models in the I r representation in order to achieve low σ fit values. The coupling between ν 17 (A″) and ν 16 (A″) resulted in many transitions with slightly perturbed frequencies, many highly displaced resonant intrastate transitions, and 165 nominal interstate transitions. Modeling the spectra of ν 17 and ν 16 required three c -axis Coriolis-coupling terms ( F ab, F ab J, and F ab K ) to treat the interaction. Many of the nominal interstate transitions form clearly discernible Q-branch bands, comprising degenerate sets of a - and b -type transitions. The rotational spectra of four higher-energy vibrationally excited states (ν 15, ν 14, ν 13, and ν 12 ), which form a complex polyad involving Coriolis and anharmonic coupling interactions, were analyzed by single-state models, thus producing only effective spectroscopic constants. Inclusion of rotationally resolved infrared transitions enabled the accurate and precise determination of vibrational band origins for the four lowest-energy fundamental states: ν 18 = 542.601 824 3 (28) cm –1, ν 17 = 665.183 128 5 (43) cm –1, ν 16 = 682.256 910 5 (43) cm –1, and ν 15 = 847.557 400 (11) cm –1 .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score0.365

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.225
Teacher spread0.220 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2024
Admission routes1
Has abstractyes

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