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Record W4402306902 · doi:10.1002/anie.202415726

Integrated “Two‐in‐One” Strategy for High‐Rate Electrocatalytic CO <sub>2</sub> Reduction to Formate

2024· article· en· W4402306902 on OpenAlexaff
Peng‐Xia Lei, Shaoqing Liu, Qi‐Rui Wen, Jiayi Wu, Shu-Wen Wu, Xiaoxiao Wei, Renfei Feng, Xian‐Zhu Fu, Jing‐Li Luo

Bibliographic record

VenueAngewandte Chemie International Edition · 2024
Typearticle
Languageen
FieldEnergy
TopicCO2 Reduction Techniques and Catalysts
Canadian institutionsCanadian Light Source (Canada)University of Toronto
FundersShenzhen Science and Technology Innovation ProgramNational Natural Science Foundation of China
KeywordsFormateAdsorptionDissociation (chemistry)SelectivityCatalysisElectrochemistryChemistryProtonationAqueous solutionMaterials scienceChemical engineeringInorganic chemistryElectrodePhysical chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract The electrochemical CO 2 reduction reaction (ECR) is a promising pathway to producing valuable chemicals and fuels. Despite extensive studies reported, improving CO 2 adsorption for local CO 2 enrichment or water dissociation to generate sufficient H* is still not enough to achieve industrial‐relevant current densities. Herein, we report a “two‐in‐one” catalyst, defective Bi nanosheets modified by CrO x (Bi−CrO x ), to simultaneously promote CO 2 adsorption and water dissociation, thereby enhancing the activity and selectivity of ECR to formate. The Bi−CrO x exhibits an excellent Faradaic efficiency (≈100 %) in a wide potential range from −0.4 to −0.9 V. In addition, it achieves a remarkable formate partial current density of 687 mA cm −2 at a moderate potential of −0.9 V without iR compensation, the highest value at −0.9 V reported so far. Control experiments and theoretical simulations revealed that the defective Bi facilitates CO 2 adsorption/activation while the CrO x accounts for enhancing the protonation process via accelerating H 2 O dissociation. This work presents a pathway to boosting formate production through tuning CO 2 and H 2 O species at the same time.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.279
Teacher spread0.260 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations63
Published2024
Admission routes1
Has abstractyes

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