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Record W4405415010 · doi:10.26434/chemrxiv-2024-5ss7j

Bias Enhanced Electro-Photocatalysis on TiO2 Nanoporous Materials for Decomposition of Forever Chemicals in Saltwater

2024· preprint· en· W4405415010 on OpenAlexafffund
Sapanbir S. Thind, Bobby A Ryane, John Hayden, Ian C. Chagunda, Mathias Paul, Jackie Hayden, J. Scott McIndoe

Bibliographic record

VenueChemRxiv · 2024
Typepreprint
Languageen
FieldEnvironmental Science
TopicWater Quality Monitoring and Analysis
Canadian institutionsUniversity of Victoria
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsPhotocatalysisNanoporousDecompositionEnvironmental scienceNanotechnologyMaterials scienceEnvironmental chemistryChemical engineeringChemistryEngineeringCatalysisOrganic chemistry

Abstract

fetched live from OpenAlex

In this study, a TiO2-based bias-enhanced photocatalytic system was prepared with the aim of achieving high photocatalytic activity in deionized as well as in saltwater systems. Highly ordered TiO2 nanoporous materials were fabricated via a double-anodization method. A small potential bias was applied that suppresses electron-hole recombination and deters interference from the ions present in the solution while minimizing electrochemical reactions. Photodegradation reactions involving Rhodamine B (RhB) were conducted to evaluate the efficacy of the nanomaterials with and without the applied bias. Our experimental results revealed that the synthesized TiO2 nanomaterials possessed high photochemical activity under UVA light, substantially enhanced with the applied bias. A very significant enhancement was observed when the Bias Enhanced Electrolytic Photocatalysis (BEEP) system was used in saline solutions. Higher photocatalytic efficiency was achieved with the increase in the salinity level in the reaction mixture. These bias-enhanced nanomaterials were successfully tested for the degradation of per- and polyfluorinated substances (PFAS), recognized as a significant threat to the environment and human health. The results indicated that the presented technology could eliminate a wide range of fluorinated molecules. The simplicity, efficacy and scalability of the new BEEP approach described in this study make the use of TiO2-based advanced oxidation process (AOP) possible in designing high-performance water purification technologies applicable to fresh and salt water.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.026
GPT teacher head0.301
Teacher spread0.274 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2024
Admission routes2
Has abstractyes

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