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Record W4407587691 · doi:10.1016/j.jcis.2025.02.077

Core/shell 1T/2H-MoS2 nanoparticle induced synergistic effects for enhanced hydrogen evolution reaction

2025· article· en· W4407587691 on OpenAlexafffund
Driss Mouloua, Thomas Vicart, Nitul S. Rajput, Bouchra Asbani, M. El Marssi, My Alı El Khakani, Mustapha Jouiad

Bibliographic record

VenueJournal of Colloid and Interface Science · 2025
Typearticle
Languageen
FieldMaterials Science
Topic2D Materials and Applications
Canadian institutionsInstitut National de la Recherche Scientifique
FundersNatural Sciences and Engineering Research Council of CanadaHereditary Disease Foundation
KeywordsNanoparticleShell (structure)Core (optical fiber)HydrogenChemistryChemical engineeringMaterials scienceNanotechnologyOrganic chemistryComposite materialEngineering

Abstract

fetched live from OpenAlex

This study investigates the photoelectrochemical potential of 1T/2H-MoS 2 nanoparticles synthesized via chemical vapor deposition. The 60 nm nanoparticles, analyzed using SEM, XRD, Raman spectroscopy, and XPS, have a high-quality mixed-phase composition. TEM revealed a core–shell structure. A MoS 2 /p-Si photocathode showed a current density of −13.5 ± 1 mA/cm 2 at 0 V and an onset potential of 110 mV, with rapid photoresponse times and an 8 % IPCE at 450 nm. The mixed-phase and core–shell structure enhance electronic and catalytic properties, promising advancements in renewable energy technologies. Green hydrogen is a highly sought-after clean fuel for the next generation of engines aimed at achieving net-zero emissions. Herein, we design and fabricate a mixed-phase core/shell nanoparticles consisting of a semiconducting 2H-MoS 2 core and a metallic 1T-MoS 2 coating. The core/shell exhibits spherical morphology with an average diameter of 60 nm. To leverage this unique structure, we develop a photocathode device composed of 1T/2H-MoS 2 core/shell integrated with p-type silicon to catalyze hydrogen evolution reaction via water splitting driven by solar energy. The core/shell device demonstrates, at zero bias, a remarkable current density of −13.5 ± 1 mA/cm 2 and an onset potential of 110 mV. Additionally, the device exhibited a rapid photoresponse time and a high incident photon-to-current efficiency reaching 80 % at 450 nm. Our findings highlight the synergistic effect of 1T/2H-MoS 2 mixed-phase core/shell structure in developing the next generation of high-efficient photocatalysts for green hydrogen generation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.014
Threshold uncertainty score0.332

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.310
Teacher spread0.293 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations18
Published2025
Admission routes2
Has abstractyes

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