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Optimization of the effect of cold plasma treatment on UAE-NADES green extraction of chickpea roots (Cicer arietinum) bioactive compounds

2025· article· en· W4407852703 on OpenAlexaff
Waseem Khalid, Imed E Benmebarek, Sina Zargarchi, Prashant Kumar, Miral Javed, Andrés Moreno, Aanchal Sharma, Gulzar Ahmad Nayik, Tuba Esatbeyoglu

Bibliographic record

VenueUltrasonics Sonochemistry · 2025
Typearticle
Languageen
FieldMaterials Science
TopicNanocomposite Films for Food Packaging
Canadian institutionsUniversity of Guelph
FundersJunta de Comunidades de Castilla-La ManchaUniversidad de Castilla-La ManchaEuropean Social FundGottfried Wilhelm Leibniz Universität Hannover
KeywordsDPPHExtraction (chemistry)NutraceuticalResponse surface methodologyChemistryRaw materialFood scienceAntioxidantChromatographyOrganic chemistry

Abstract

fetched live from OpenAlex

The chickpea (Cicer arietinum L.) root is an agricultural by-product with the potential for extracting valuable bioactive compounds that often remains underutilized. This study introduces an integrated extraction methodology to enhance the extraction of bioactives using atmospheric air low-pressure cold plasma (CP) treatment followed by ultrasound-assisted extraction (UAE) with natural deep eutectic solvents (NADES). Chickpea root powder was first subjected to CP treatment under optimized conditions (power, pressure, and time) identified via response surface methodology (RSM). Subsequently, UAE-NADES extraction was performed to maximize the results of antioxidant activity (DPPH) and total phenolic content (TPC). The integrated CP-UAE-NADES process enhanced TPC and DPPH compared to the untreated sample (non-CP). The optimum conditions were 11.5 min, 52 W, and 0.65 mbar. The predicted values of the Box-Behnken design for TPC and DPPH were compatible with the experimental Furthermore, microbial load reduction and color stability were analyzed to ensure chickpea root quality and functionality. The combined extraction methodology offers a sustainable and eco-friendly approach for the valorization of chickpea root as a source of bioactives, with potential applications in functional foods, nutraceuticals, and pharmaceuticals.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.016
Threshold uncertainty score0.723

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.247
Teacher spread0.241 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations14
Published2025
Admission routes1
Has abstractyes

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