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Record W4408045224 · doi:10.1021/acsomega.4c10782

Glassy Fluorene and Sulfone Polyesters with High Refractive Index and Thermal Stability Whose Monomers Induce Estrogenic Bioactivity

2025· article· en· W4408045224 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueACS Omega · 2025
Typearticle
Languageen
FieldChemistry
TopicPhotopolymerization techniques and applications
Canadian institutionsInnovation Cluster (Canada)
FundersUniversity of Central Florida
KeywordsPolyesterFluoreneThermal stabilitySulfoneMonomerPolymer chemistryMaterials scienceRefractive indexChemistryOrganic chemistryPolymerOptoelectronics

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Two new diacid monomers containing either fluorene or sulfone moieties polymerize via step-growth polymerization in the presence of their diol counterparts or alkyl diols (ethylene glycol and 1,6-hexanediol), forming eight new cardo structure polyesters. The polymers exhibit high optical transparency in the thin-film form with refractive indices ranging from 1.56 to 1.69, tunable glass transition temperatures from ca. 40 to 116 °C with no melting temperature, and resistance to thermal degradation in a nitrogenous atmosphere, reaching 350–398 °C before observing 10% weight loss. Their molecular weights, M w, range from ca. 17 to 77 kDa, with an average polydispersity, Đ, of 1.5, and average purified yields of 82%. The polymers absorb light primarily in the UV region from ca. 228 to 320 nm with no absorption from 320 to 800 nm. A critical finding is that some of the fluorene and sulfone monomers induce negative bioactivity and even cell death in T47D-KBLuc cells, a breast cancer cell line, at high concentrations. This report details the project inspiration, monomer synthesis, polymerization steps, structural confirmation, material characterization, and the impact of the new monomer’s estrogenic and antiestrogenic bioactivity.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.022
Threshold uncertainty score0.599

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.230
Teacher spread0.222 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it