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Record W4408202758 · doi:10.1021/acsnano.4c15960

Dynamic Lithium Transport Pathway via Crack Formation in Phase-Separating Battery Particles

2025· article· en· W4408202758 on OpenAlexaff
Chihyun Nam, Bonho Koo, Juwon Kim, Jinkyu Chung, Jaejung Song, Danwon Lee, Sungjae Seo, Munsoo Song, Namdong Kim, Markus Weigand, Jian Wang, Jongwoo Lim

Bibliographic record

VenueACS Nano · 2025
Typearticle
Languageen
FieldEngineering
TopicAdvancements in Battery Materials
Canadian institutionsCanadian Light Source (Canada)
FundersNational Research Foundation of Korea
KeywordsMaterials scienceLithium (medication)Battery (electricity)Stress (linguistics)Particle (ecology)Phase (matter)Composite materialChemistryPhysics

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Nanoscale cracks within battery particles are ubiquitously induced during battery cycling. Tracking the origin of nanocrack formation and its subsequent propagation remains challenging, although it is crucial for the cycle life and kinetics of batteries. Moreover, it is even more challenging to understand how such nanocracks influence lithium (de)insertion pathways and local strain fields within battery particles. In this study, we utilized operando scanning transmission X-ray microscopy on individual LiFePO 4 (LFP) particles to visualize the relationship between lithium (de)insertion pathways and crack formation and propagation. We first demonstrate the generation mechanism of nanocracks occurs when the lithium insertion pathway at the edge of fresh LFP particles induces strong tensile stress in the middle of the particle. Then, we directly observe the nanocrack propagation mechanism, where the freshly exposed surface near the crack activates a fast lithium (de)insertion pathway, completely altering the internal stress fields near the nanocrack. Once the nanocrack transforms the dynamic lithium pathway and distribution, the delithiation process induces crack-opening tensile stress, while the lithiation process generates crack-closing compressive stress. 3D phase-field simulations support these observations, showing how dynamic lithium distribution shapes stress fields. Our findings reveal a recursive chemo-mechanical loop involving lithium (de)insertion pathways, internal stress fields, and crack development.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.059
Threshold uncertainty score0.581

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.263
Teacher spread0.253 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations12
Published2025
Admission routes1
Has abstractyes

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