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Record W4408490090 · doi:10.5194/egusphere-egu25-19039

From the weakest to strongest sulphide: how the strength of pyrite evolves during deformation

2025· preprint· en· W4408490090 on OpenAlexaff
Rellie M. Goddard, Thomas Breithaupt, Noah Phillips, Tarryn Cawood, Brendan Dyck, Crystal LaFlamme, D. J. Wallis, Pete Hollings, Harison S. Wiesman

Bibliographic record

Venuenot available
Typepreprint
Languageen
FieldEnvironmental Science
TopicMinerals Flotation and Separation Techniques
Canadian institutionsLakehead University
Fundersnot available
KeywordsPyriteDeformation (meteorology)GeologyGeochemistry

Abstract

fetched live from OpenAlex

Sulphides are common host minerals for trace elements, including critical and precious metals, and are widely associated with a range of ore deposit types. Recent work on natural sulphides has highlighted the link between the motion of dislocations—lattice defects that act as carriers of deformation—and the transport of trace elements through mechanisms such as pipe diffusion, in which dislocations act as fast diffusion pathways, or the correlated motion of dislocations and impurities, whereby impurities are entrained within the stress field of migrating dislocations. Despite the clear influence of deformation on the distribution of trace and precious metals and, therefore, on the economic viability of an orebody, the strengths of different sulphides are not well constrained. Flow laws for sulphides either do not exist or are not able to reproduce ductile flow, with experiments instead ending in brittle failure. This paucity of experimental studies makes interpreting natural microstructures challenging. In this work, we start by constraining the relative strengths and hardening behaviours of three sulphides, pyrite, sphalerite, and chalcopyrite, via nanoindentation experiments at room temperature. Through subsequent characterisation of the microstructures using electron backscatter diffraction and the concentration of trace elements and critical- and precious metals using LA-ICP-MS, we explore how grain size, orientation, and chemistry affect mineral strength. Although pyrite is widely considered to be stronger than other common sulphides, our data suggest that the intrinsic yield stress of pyrite may, surprisingly, be weaker than the yield stress of both chalcopyrite and sphalerite. However, as deformation proceeds and the density of geometrically necessary dislocations (GNDs) is elevated pyrite strengthens rapidly. These results suggest a strong size effect at low temperature in which elastic dislocation interactions are stronger within pyrite compared to other sulphides. Our results are consistent with observations of fine-grained pseudo-porphyroclasts in nature, for which the GND density is predicted to be inversely proportional to the grain size. Overall, this work provides a foundation for accurate models of how the strength of pyrite evolves and, as such, how transport of trace elements and upgrading of ore deposits may proceed.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.009

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0010.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.259
Teacher spread0.242 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designObservational
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes1
Has abstractyes

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