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Record W4410586107 · doi:10.46770/as.2025.005

Laser-induced Breakdown Spectroscopy (LIBS) in the Field: How Rock Moisture Influences Spectral Quality and Plasma Properties

2025· article· en· W4410586107 on OpenAlex
Samira Selmani, François Vidal

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

fundA Canadian funder is recorded on the work.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueAtomic Spectroscopy · 2025
Typearticle
Languageen
FieldEngineering
TopicLaser-induced spectroscopy and plasma
Canadian institutionsnot available
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsLaser-induced breakdown spectroscopyChemistrySpectroscopyPlasmaMoistureField (mathematics)Quality (philosophy)Spectral propertiesLaserAnalytical Chemistry (journal)Environmental chemistryOpticsNuclear physicsComputational chemistryPhysics

Abstract

fetched live from OpenAlex

Before LIBS can be applied to analysis at mine sites under normal weather conditions, a number of practical issues need to be addressed.One of these is the moisture content of rock samples taken directly in the field.To assess the effect of rock moisture content on LIBS measurements, we studied its temporal evolution as the rock dried under ambient laboratory conditions using a series of 1080 laser shots (18 rows 60 columns) at 2 Hz (8 ns pulse duration, 1064 nm wavelength, with a fluence of ~4 kJ cm -2 ).At maximum moisture, the LIBS spectra are weak, with only a few strong lines emerging from the background noise, while a richer spectrum appears as the rock dries.Color maps of LIBS spectra averaged over wavelength (white light) from the rock surface and net H line intensity from the water layer form complex, weakly correlated mosaics whose components depend on local rock properties (e.g., composition, porosity, asperities).However, the time evolution of their average over each of the 18 rows correlates well with that of the rock weight and microwave moisture measurements.Using the H line broadening and the ratio between the Mg II 280.27 nm and Mg I 285.21 nm line, the space and time averaged plasma produced in both the dry and wet rock areas is characterized by an electron number density in the range of 10 17 cm -3 and an ionization temperature close to 1 eV.The physical mechanisms involved are discussed.This study highlights the importance of controlling the moisture of the rock at the mining site before starting LIBS measurements, as it has a significant impact on the accuracy of the results obtained.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.014
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.268
Teacher spread0.252 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it