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Record W4411135780 · doi:10.1021/jacs.5c04222

Molecular-Level Tailoring of Energy Structure in Ternary Conjugated Polymers with a Built-in Ru-Complex Catalyst for Efficient CO<sub>2</sub> Reduction Photocatalysis

2025· article· en· W4411135780 on OpenAlexaff
Kotaro Ishihara, Akinobu Nakada, Hajime Suzuki, Akira Yamakata, Osamu Tomita, Akinori Saeki, Ryu Abe

Bibliographic record

VenueJournal of the American Chemical Society · 2025
Typearticle
Languageen
FieldEnergy
TopicAdvanced Photocatalysis Techniques
Canadian institutionsCarbon Engineering (Canada)
FundersPrecursory Research for Embryonic Science and TechnologyJapan Society for the Promotion of Science
KeywordsPhotocatalysisTernary operationCatalysisChemistryConjugated systemNanotechnologyVisible spectrumPhotochemistryPolymerChemical engineeringCombinatorial chemistryOptoelectronicsMaterials scienceOrganic chemistry

Abstract

fetched live from OpenAlex

Efficient catalytic CO 2 conversion by harnessing visible-light energy is a substantial challenge for sustainability. Photocatalytic materials consisting of light absorbers and catalysts have been extensively developed. However, efficient photocatalytic systems have so far relied on the use of precious metal-based compounds or materials as light-absorbing components, primarily because of their long-lived photoexcited states. Herein, we report the design principles of ternary conjugated polymers as a metal-free light absorber with a built-in metal complex catalyst for substantially activating CO 2 reduction photocatalysis. The ternary conjugated system enabled exceedingly flexible tuning of their energy structure, which is beneficial for long-range charge separation by manipulating the photoexcited electrons to the site-selectively introduced molecular catalyst center. The key cascade energy structure was tailored, and its impacts on photocatalysis were unveiled by using both spectroscopic experiments and theoretical calculations. The precise molecular design resulted in very active visible-light CO 2 reduction, even without the aid of a precious metal-based light absorber, recording an external quantum efficiency up to 32.2% and producing a concentrated formate (∼0.48 M).

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.262
Teacher spread0.253 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations9
Published2025
Admission routes1
Has abstractyes

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Same venueJournal of the American Chemical SocietySame topicAdvanced Photocatalysis TechniquesFrench-language works237,207