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Record W4411278968 · doi:10.26434/chemrxiv-2025-l4mc6

Supramolecular topological adhesion boosts delamination resistance in carbon fiber reinforced polymers

2025· preprint· en· W4411278968 on OpenAlex
Enrico Dalcanale, Silvia D’Auria, Francesco Bertocchi, Alice Boschetti, Andrea Lapini, Alberto Fina, Alessandro Pedrini, Roberta Pinalli, C. Pernechele

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueChemRxiv · 2025
Typepreprint
Languageen
FieldEngineering
TopicFiber-reinforced polymer composites
Canadian institutionsDalsa Corporation
FundersMinistero dell'Università e della RicercaUniversità degli Studi di ParmaMinistero dell’Istruzione, dell’Università e della RicercaEuropean CommissionDipartimenti di Eccellenza
KeywordsMaterials scienceSupramolecular chemistryDelamination (geology)AdhesionComposite materialSupramolecular polymersPolymerFiberPolymer scienceChemistryMoleculeOrganic chemistryPaleontologyGeology

Abstract

fetched live from OpenAlex

In this study, we introduce supramolecular topological adhesion as an innovative and effective methodology to enhance interlaminar fracture toughness in carbon fiber reinforced polymers (CFRPs). We achieved remarkable improvements in delamination resistance by physically entangling phenoxy resins within an epoxy matrix and introducing sacrificial H-bond interactions via ODIN (1-(7-Oxo-7,8-Dihydro-1,8-Naphthyridin-2-yl)urea) units. The ODIN units form sextuple H-bonding dimers in the cured epoxy matrix among plies, experimentally quantified via UV-Vis spectroscopy, whose detachment hinders crack propagation. The viability of this approach was tested using various phenoxy resins with different molecular weights and with different levels of ODIN functionalization. Single lap shear (SLS) tests demonstrated a notable increase in adhesion strength, sorting out PKHB-ODIN 13% as the best candidate as interlaminar adherent. Delamination resistance was determined through double cantilever beam (DCB) and end-notched flexure (ENF) tests, showing up to 120% and 80% increases in Mode I and Mode II fracture toughness, respectively. The limited DCB and ENF test increments observed for control adherent PKHB-PU 23% functionalized with phenylurea (PU) groups, demonstrates that the strength of topological H-bonding is pivotal to boost delamination resistance. The results indicate that this method holds great potential for improving the durability of CFRP composites, especially in applications requiring high resistance to delamination.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.438
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.222
Teacher spread0.214 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it