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Record W4411332597 · doi:10.1021/acs.macromol.5c00768

Force-Accelerated Ring Opening of Episulfide by Pulsed Ultrasonication

2025· article· en· W4411332597 on OpenAlexaff
Chang-Sik Ko, H. P. Wang, Van‐Sieu Luc, Chunyi Hsu, Yangju Lin, Yu-Wen Huang, Chia‐Chih Chang

Bibliographic record

VenueMacromolecules · 2025
Typearticle
Languageen
FieldChemistry
TopicInorganic and Organometallic Chemistry
Canadian institutionsUniversity of Waterloo
FundersNational Science and Technology Council
KeywordsSonicationRing (chemistry)ChemistryMaterials scienceOrganic chemistryChromatography

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Covalent polymer mechanochemistry is an emerging field that leverages the mechanical force transduced by polymer chains to bias or alter the reaction pathways uniquely, thereby influencing the stereoselectivity of chemical transformations. This study investigates the mechanochemical reactivities of episulfides featuring alkyl, ester, and phenyl substituents under pulsed ultrasonication, and the results demonstrate that episulfides bearing alkyl and phenyl substituents can undergo C–C bond cleavage to produce reactive intermediates that are amenable to subsequent cis – trans isomerization and cycloaddition reactions. In contrast, the episulfide with ester substituents is mechanochemically inactive.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.109
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.238
Teacher spread0.230 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2025
Admission routes1
Has abstractyes

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