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Record W4412472519 · doi:10.26434/chemrxiv-2025-xjdm7

Pentavalent Ta-Substitution Enhances Ionic Conductivity and Critical Current Density in NASICON for Sodium-Ion Batteries

2025· preprint· en· W4412472519 on OpenAlexafffund
Vishal Ranawade, Deepak Kumar Gorai, M. Dinachandra Singh, Kanwar Singh Nalwa, Raju Kumar Gupta, Lingzi Sang, Sudarshan Narayanan

Bibliographic record

VenueChemRxiv · 2025
Typepreprint
Languageen
FieldEngineering
TopicAdvancements in Battery Materials
Canadian institutionsUniversity of Alberta
FundersCanada Foundation for InnovationDepartment of Science and Technology, Ministry of Science and Technology, IndiaIndian Institute of Technology KanpurUniversity of AlbertaNatural Sciences and Engineering Research Council of CanadaGovernment of Alberta
KeywordsElectrolyteFast ion conductorConductivityIonic conductivityCurrent densityMaterials scienceIonSodiumVacancy defectChemistryAnalytical Chemistry (journal)Inorganic chemistryChemical engineeringElectrodePhysical chemistryCrystallographyMetallurgyOrganic chemistry

Abstract

fetched live from OpenAlex

NASICONs are promising electrolyte candidates for all-solid-state sodium-ion batteries. In this study, we report a Ta-substituted NASICON electrolyte, Na3.32Zr1.92Ta0.08Si2.4P0.6O12 (8Ta-NZSP2.4), which exhibits a high room temperature Na+ conductivity of 4.26 mS·cm-1. Na|8Ta-NZSP2.4|Na cell shows over 250 stable cycles at a 0.1 mA·cm-1 current density while maintaining low overpotentials (<20 mV) and no soft shorting, outperforming the symmetric cell containing unsubstituted NZSP2.4, which soft-shorted at cycle 40. Upon Ta-substitution, the critical current density of NZSP2.4 increased from 0.3 to 0.7 mA·cm-1. A Na₃V₂(PO₄)₃|8Ta-NZSP2.4|Na full cell retained 89.5% of the specific capacity when operating at 0.3C for 100 cycles at room temperature with no additional stack pressure applied. Our complementary DFT calculation shows an increased Na+ vacancy and the presence of a correlated migration pathway in Ta-substituted NZSP2.4, which ultimately enabled a reduced energy barrier for Na+ transport. The combined experimental and theoretical study underpinned the design principle of pentavalent substituted NASICONs for promoting Na+ conductivity.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.040
GPT teacher head0.319
Teacher spread0.279 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes2
Has abstractyes

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