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Record W4412641847 · doi:10.1021/acs.analchem.5c03412

Open Type Solid Photoacoustic Trace Gas Sensor with Multi-Pass Absorption Enhancement

2025· article· en· W4412641847 on OpenAlexafffund
J.Y Zhang, Lixian Liu, Jialiang Sun, Xueshi Zhang, Baisong Chen, Yize Liang, Binxing Zhao, Huiting Huan, Xuesen Xu, Huailiang Xu, Andreas Mandelis

Bibliographic record

VenueAnalytical Chemistry · 2025
Typearticle
Languageen
FieldChemistry
TopicSpectroscopy and Laser Applications
Canadian institutionsUniversity of Toronto
FundersFundamental Research Funds for the Central UniversitiesNatural Sciences and Engineering Research Council of CanadaNational Natural Science Foundation of China
KeywordsChemistryTrace gasAbsorption (acoustics)Analytical Chemistry (journal)Attenuation coefficientSIGNAL (programming language)Time delay and integrationWavelengthPhotoacoustic spectroscopyPath lengthDetection limitOpticsRadiative transferLaser

Abstract

fetched live from OpenAlex

A wavelength modulation solid photoacoustic spectroscopic (WM-SPAS) sensor enhanced with an open-type multi-pass cell (OMPC) is reported for highly sensitive detection of trace gases, especially suitable for highly corrosive and long optical-to-thermal (non-radiative) relaxation gaseous species. Such open configuration is quite different from traditional trace gas detection methods in that the separation design of the acoustic signal detector and gas absorption cavity avoids the adversely corrosive effect and reduces signal fluctuations caused by high flow rates. The modulated beam after the optical absorption by the target gas in the designed open-type multi-pass path is directed into a self-designed solid chamber, filled with carbon powder while the photoacoustic (PA) pressure signal is analyzed to yield the target gas concentration. By optimizing the incident beam angle, the OMPC achieves 96 reflections, yielding a 9.6 m optical path length enhancement. Using acetylene (C 2 H 2 ) as a test sample and a DFB laser as the excitation source, this WM-SPAS sensor achieves sensitivity of 80 ppb and corresponding normalized noise equivalent absorption coefficient equal to 2.42 × 10 –9 cm –1 W/Hz –1/2 with 1 s time constant and modulation frequency as low as 39 Hz, which enables the sensor to detect gases with slow non-radiative relaxation. An Allan deviation analysis indicated the minimum detection limit could be further improved to 7 ppb at 100 s integration time. The response deviation of the PA signal under different flow rates was characterized by a coefficient of variation of 0.71‰. With its separate structure design, this newly developed PAS trace gas sensor offers unique advantages for open trace gas detection in high-flow and corrosive environments.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.326
Teacher spread0.308 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2025
Admission routes2
Has abstractyes

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