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Aerobic biodegradation of 3D printed biocomposites containing polylactic acid and industrial residual forest biomass

2025· article· en· W4413007127 on OpenAlexafffund
Sarra Helaoui, Ahmed Koubaa, Hédi Nouri, Martin Beauregard, Sofiane Guessasma

Bibliographic record

VenueChemosphere · 2025
Typearticle
Languageen
FieldMaterials Science
Topicbiodegradable polymer synthesis and properties
Canadian institutionsUniversité du Québec en Abitibi-Témiscamingue
FundersRES’EAU-WaterNETFonds de recherche du Québec – Nature et technologiesCanada Excellence Research Chairs, Government of CanadaMitacsAgence Nationale de la RechercheCanada Research ChairsNatural Sciences and Engineering Research Council of CanadaFonds de recherche du Québec
KeywordsPolylactic acidBiodegradationBiomass (ecology)Pulp and paper industryResidualWaste management3d printedEnvironmental scienceChemistryOrganic chemistryEngineeringEcologyBiologyManufacturing engineeringPolymer

Abstract

fetched live from OpenAlex

This study investigates the biodegradation of 3D printed biocomposites under aerobic composting conditions. Biodegradable containers were prepared using forest biomass, wood ash (WA), wood sawdust (WS), and cellulose fiber (CF), as fillers and polylactic acid (PLA) as matrix and were processed via fused filament fabrication (FFF). Biodegradability tests were conducted in a laboratory-scale installation using the compost burial method for three months. Weight loss measurements were measured every 7 days throughout testing. The physicochemical and morphological properties of the samples were characterized. Of the biocomposites, PLA with 20 wt% wood sawdust showed the highest water absorption. The kinetic mechanisms followed typical Fickian diffusion behavior. The crystallinity improved with the addition of 20 wt% cellulose fibers. PLA degrades in a two-step process. Initially, temperature and moisture break down the PLA chains into lactic acid monomers. Subsequently, microorganisms in the compost convert these compounds into carbon dioxide, water, and biomass. A 97 % PLA weight loss was achieved after 3 months, with added fillers decreasing the biodegradability rate. Cracks on the surface and color changes were noted. Microorganisms were observed to settle in the spaces between the layers created by 3D printing. Fourier transform infrared spectra, scanning electron microscope micrographs, and synchrotron X-ray microtomographs revealed a microbial biofilm layer on the sample surfaces. After biodegradation, biocomposites can serve as soil fertilizer. Therefore, 3D printed biodegradable containers offer eco-friendly solutions that help minimize agricultural plastic waste accumulation and lower greenhouse gas emissions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.001

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.026
GPT teacher head0.238
Teacher spread0.212 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2025
Admission routes2
Has abstractyes

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