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Record W4413378310 · doi:10.1021/acs.iecr.5c00826

Pressurized Chemical Looping–Steam Methane Reforming for Thermal H<sub>2</sub> Production

2025· article· en· W4413378310 on OpenAlexafffundabout
Robert T. Symonds, Rebecca Modler, Robin W. Hughes, Basil Wadi, Scott Champagne, Nicole Bond, Kelly Atkinson

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2025
Typearticle
Languageen
FieldEngineering
TopicChemical Looping and Thermochemical Processes
Canadian institutionsNatural Resources Canada
FundersOffice of Energy Research and DevelopmentNatural Resources Canada
KeywordsSteam reformingChemical looping combustionHydrogen productionMethaneMethane reformerWaste managementEnvironmental scienceProduction (economics)ThermalSyngasChemistryChemical engineeringMaterials scienceNuclear engineeringProcess engineeringHydrogenThermodynamicsFluidized bedEngineeringOrganic chemistry

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Large quantities of heat, steam, electricity, and hydrogen are required in many major industrial sectors such as oil and gas and iron and steel. However, the most common technologies for generating these products are large-scale emitters of CO 2 and at the present time must still rely on fossil fuel feedstocks. The deployment of carbon capture, utilization, and storage (CCUS) technologies will be critical in reaching both Canadian and international net-zero emissions targets by 2050. More traditional approaches for CO 2 capture, such as solvent-based scrubbing, can be implemented to reduce emissions but often fall short of attaining carbon-neutral products. Pressurized chemical looping–steam methane reforming (PCL-SMR) has the potential to produce zero-emission H 2 for combustion systems at an attractive cost, thereby avoiding the need for postcombustion CO 2 capture which can be cost prohibitive at certain scales. This is achieved by replacing the existing SMR firebox with dual-reactor chemical looping with inherent CO 2 separation. This work considers a comparison between conventional SMR with and without postcombustion CO 2 capture to that of PCL-SMR at an industrial-scale H 2 production level (∼290 t/day). In all configurations, the syngas is cooled, the H 2 product is separated via pressure swing adsorption before compression, and the tail gas is recycled into the combustion system. The captured CO 2 is processed via a cooling, drying, and compression system to meet the supercritical CO 2 transportation specifications. By operating at elevated pressures (∼6 bar(g)), zero direct CO 2 emissions are achievable without the need for costly gaseous O 2 production, while increasing the net H 2 production efficiency and lowering fresh-water consumption. A detailed comparative techno-economic analysis and life-cycle assessment show a significantly lower levelized cost of H 2 production via PCL-SMR in comparison to SMR with amine-based CO 2 capture, while achieving both greater direct (Scope 1) and indirect (Scopes 2 and 3) CO 2 emission reductions. In addition, several other key benefits of PCL-SMR beyond costs and environmental burdens are highlighted, such as a significant reduction in reformer tube stress and H 2 production efficiency.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.024
Threshold uncertainty score0.079

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0240.004

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.048
GPT teacher head0.303
Teacher spread0.255 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2025
Admission routes3
Has abstractyes

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