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Impact of nucleation temperature and hydroxyethyl starch on ice crystal growth: Implications for cell viability during extreme temperature fluctuations

2025· article· en· W4413770882 on OpenAlexafffund
Nishaka William, Anika Tahsin Rahman, Jason P. Acker

Bibliographic record

VenueJournal of Thermal Biology · 2025
Typearticle
Languageen
FieldEngineering
TopicFreezing and Crystallization Processes
Canadian institutionsCanadian Blood ServicesUniversity of Alberta
FundersCanadian Institutes of Health ResearchAlberta Innovates
KeywordsNucleationIce nucleusMaterials scienceIce crystalsStarchCrystal (programming language)Chemical engineeringEnvironmental scienceThermodynamicsChemistryMeteorologyFood sciencePhysics

Abstract

fetched live from OpenAlex

Extreme temperature fluctuations during routine handling and shipping of cryopreserved cell products significantly compromise product quality in ways that extend beyond the duration and peak temperature of the fluctuation. The type of cryoprotectant used and the initial ice nucleation temperature influence ice crystal growth during rewarming events, in turn impacting cell survival. Using a cryomicroscope together with temperature profiles recorded in cord-blood units, ice crystal growth was tracked through five transient-warming events (TWEs) that peaked at -30 °C, -20 °C, or -10 °C. Initial freezing conditions were modified either by adding 6 % (w/v) hydroxyethyl starch (HES) or by lowering the ice-nucleation temperature by 10 °C. Across five TWEs, ice-crystal area saw the greatest increase when the peak rewarming temperature was -10 °C. Although adding HES further accelerated this recrystallization, it still protected Jurkat cells after a single TWE. Lowering the nucleation temperature also improved viability in samples warmed to -20 °C, regardless of HES supplementation. These findings show that ice crystal growth is not the sole cause of injury during transient rewarming; other temperature-dependent stresses also play a role. Importantly, careful optimisation of cryoprotectant composition and nucleation temperature can bolster cellular resilience to temperature excursions, potentially reducing quality losses during the storage and transport of cryopreserved therapeutics.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.254
Teacher spread0.245 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations0
Published2025
Admission routes2
Has abstractyes

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