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Record W4413894583 · doi:10.1002/cssc.202501550

Platinum‐Doped Carbon Nitride‐Loaded Poly( <i>N</i> ‐Isopropylacrylamide) Hydrogel Thin Films for Green Hydrogen Production Systems: Morphological Study for Higher Efficiency

2025· article· en· W4413894583 on OpenAlexafffund
Morgan P. Le Dû, David P. Kosbahn, Thomas Baier, Julija Reitenbach, Qi Zhong, Apostolos Vagias, R. Cubitt, Narendra Chaulagain, Karthik Shankar, Hagen Übele, Katharina Krischer, Peter Müller‐Buschbaum

Bibliographic record

VenueChemSusChem · 2025
Typearticle
Languageen
FieldEnergy
TopicAdvanced Photocatalysis Techniques
Canadian institutionsUniversity of Alberta
FundersCenter for NanoScience, Ludwig-Maximilians-Universität MünchenBayerisches Staatsministerium für Wissenschaft, Forschung und KunstMitacsBundesministerium für Forschung und TechnologieChina Scholarship CouncilDeutsche Forschungsgemeinschaft
KeywordsPhotocatalysisCatalysisGraphitic carbon nitrideMaterials scienceHydrogen productionChemical engineeringThin filmCarbon nitrideSelf-healing hydrogelsPlatinumNanotechnologyChemistryPolymer chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Photocatalytic water splitting enables the generation of green hydrogen (H 2 ). In this framework, water and sunlight are the sustainable sources. Photocatalyst‐loaded hydrogel materials have already shown their potential as a water storage and catalyst host matrix for H 2 production. This study explores the thin film geometry of such systems to demonstrate the scalability of photocatalysis. Graphitic carbon nitride is used as a catalyst and combined with platinum as a co‐catalyst. The resulting catalytic centers are introduced in poly( N ‐isopropylacrylamide) hydrogel thin films. First, the swelling behavior of the resulting hybrid hydrogels is studied under high relative humidity, and the influence of different catalyst loadings is discussed. Then, time‐of‐flight neutron reflectometry is used to access the vertical material composition inside the hybrid thin film in the dry state, which shows an enrichment layer of catalyst at the substrate–bulk interface. Operando grazing incidence small‐angle neutron scattering displays the microscopic changes happening under heavy water (D 2 O) vapor and light irradiation. Next, gas chromatography demonstrates the potential of the studied hydrogel films by determining their H 2 production rates. The recorded H 2 production is correlated to the microstructure analysis and reveals the importance of the observed catalyst enrichment layer.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.007
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.283
Teacher spread0.261 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes2
Has abstractyes

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