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Record W4414017958 · doi:10.1021/acsami.5c15495

Toward Glioblastoma Treatment with High Spatiotemporal Precision: Controlling Temozolomide Release from Upconverting Nanoparticles Using Near-Infrared Light

2025· article· en· W4414017958 on OpenAlexafffund
Vivienne Tam, А. Н. Орлов, Mingrui Guo, Fiorenzo Vetrone, Marta Cerruti

Bibliographic record

VenueACS Applied Materials & Interfaces · 2025
Typearticle
Languageen
FieldEngineering
TopicNanoplatforms for cancer theranostics
Canadian institutionsInstitut National de la Recherche ScientifiqueMcGill University
FundersFonds de recherche du Québec – Nature et technologiesNatural Sciences and Engineering Research Council of CanadaCanada Research Chairs
KeywordsMaterials scienceTemozolomideGlioblastomaNanoparticleInfraredPhoton upconversionNanotechnologyOptoelectronicsCancer researchOpticsLuminescenceMedicine

Abstract

fetched live from OpenAlex

As the first-line chemotherapeutic for glioblastoma multiforme (GBM), Temozolomide (TMZ) suffers from rapid degradation in physiological fluid, making it difficult to deliver sufficient doses of active TMZ to GBM tumors without inducing severe side effects. By protecting TMZ and then controlling its release using an external stimulus, we can prevent its premature degradation, thereby increasing its active concentration at the tumor site. Here, we present a near-infrared (NIR) controlled system in which TMZ is protected within a polymer before its on-demand release. NIR light is preferable, given its high penetration depth and noncarcinogenicity, but ultraviolet (UV) light is required to cleave chemical bonds. Upconverting nanoparticles (UCNPs) overcome this challenge as they convert NIR to UV, a property of the rare-earth lanthanides of which they are comprised. In this work, we coat UCNPs with poly(acrylic acid) (PAA) conjugated to a UV-cleavable nitrobenzyl photolinker (PhL) covalently linked to TMZ and show that this UCNP@PAA-PhL-TMZ system releases TMZ under low laser power (1 W/cm 2 ) NIR, with 100% release after 30 min irradiation. When a 5 min NIR pulse was used to trigger TMZ release after NP internalization into U87MG GBM cells, we observed significant cell death after 24 h, even at concentrations an order of magnitude lower than current TMZ tumor concentrations, with multiple pulses inducing a larger effect. This work highlights the importance of drug release after cellular internalization and is a key step toward enhancing TMZ effectiveness as well as developing a tool to administer time-sensitive treatments personalized to individual GBM patients.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.215
Teacher spread0.205 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes2
Has abstractyes

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