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Record W4414265377 · doi:10.1021/acssensors.5c02104

Dual-Chronoamperometry Drift Correction for Electrochemical Sensors

2025· article· en· W4414265377 on OpenAlexaff
Kimberly T. Riordan, Kefan Yang, Ethan Brazelton, Mohammed Eslami, Ashley Copenhaver, Fatemeh Esmaeili, Connor D. Flynn, Zhenwei Wu, Scott E. Isaacson, Dingran Chang, Maria D. Cabezas, Vuslat B. Juska, Jagotamoy Das, Edward H. Sargent, Shana O. Kelley

Bibliographic record

VenueACS Sensors · 2025
Typearticle
Languageen
FieldChemical Engineering
TopicAnalytical Chemistry and Sensors
Canadian institutionsUniversity of Toronto
FundersH2020 Marie Skłodowska-Curie ActionsDefense Sciences Office, DARPADivision of Graduate EducationInternational Institute for Nanotechnology, Northwestern University
KeywordsChronoamperometrySIGNAL (programming language)Sensitivity (control systems)Reliability (semiconductor)Capacitive sensingFaradaic currentMonolayerKalman filterSolution of Schrödinger equation for a step potential

Abstract

fetched live from OpenAlex

Accurate sensing of biomolecular targets is crucial for diagnosing diseases and developing technologies for personalized medicine. However, measuring biomarker levels with high precision is often challenging due to signal drift caused by biofouling and monolayer instability. We demonstrate a novel continuous dual-chronoamperometry method with faradaic current extraction to enable accurate and reliable detection of biomarkers in the presence of drift. We apply two sequential chronoamperometry pulses, a reference (-500 mV) and a test (+500 mV), to capture all capacitive and faradaic currents in the range. In the absence of the target, the drift in the reference and test currents is multilinear, and this relationship can be used to predict the contribution of the target current. As a proof-of-concept, we demonstrate that signal drift can be corrected using our molecular pendulum for IFN-γ detection. Importantly, we show that this technique is broadly applicable to other amperometry-based systems such as a monolayer transporter sensor, an electrochemical DNA sensor, and electrochemical aptamer-based sensors. Moreover, we train a linear regression machine learning model and use its error to quantify target concentrations with dual-chronoamperometry data. This novel method enhances the reliability and sensitivity of chronoamperometry, paving the way for its application in real-time monitoring scenarios.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.006
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Methods · Consensus signal: Methods
Teacher disagreement score0.002
Threshold uncertainty score0.013

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0020.006
Meta-epidemiology (narrow)0.0020.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0010.001
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0020.001
Research integrity0.0020.003
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.245
Teacher spread0.238 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreMethods

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations8
Published2025
Admission routes1
Has abstractyes

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