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Record W4415452711 · doi:10.1021/acsestwater.5c00375

Development of a Method for Assessing Illicit Drug Consumption during Brazilian Carnival through Wastewater-Based Epidemiology Using Gas Chromatography–Mass Spectrometry

2025· article· en· W4415452711 on OpenAlexaff
Ana Flávia B. de Oliveira, Aline de Melo Vieira, Pedro Gabriel C. de Lucena, Bruna Ramos de Souza Gomes, Thayane Cristina da S. Moreira, Ignes Regina dos Santos, Kauê de Oliveira Chinaglia, José Luiz Costa, Jandyson M. Santos

Bibliographic record

VenueACS ES&T Water · 2025
Typearticle
Languageen
FieldPharmacology, Toxicology and Pharmaceutics
TopicForensic Toxicology and Drug Analysis
Canadian institutionsIONICS Mass Spectrometry (Canada)
FundersFundação de Amparo à Ciência e Tecnologia do Estado de PernambucoConselho Nacional de Desenvolvimento Científico e TecnológicoCoordenação de Aperfeiçoamento de Pessoal de Nível SuperiorFundação de Amparo à Pesquisa do Estado de São Paulo
KeywordsIllicit drugCannabisMDMAEcstasyMephedroneRecreational DrugDrugStimulantConsumption (sociology)

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Wastewater-based epidemiology (WBE) is a noninvasive and real-time method for assessing illicit drug consumption and the impact of events on community drug use. In this study, a WBE method combining solid-phase extraction (SPE) and gas chromatography–mass spectrometry (GC-MS) was applied to monitor assessing illicit drugs in raw wastewater samples, which were collected during the 2023 Carnival, and in a reference week in Recife (community A) and Olinda (community B) cities. The method was then validated for linearity, limit of quantification, precision, and accuracy. Population-normalized daily drug loads followed the consumption trend of cannabis > cocaine > MDMA > methamphetamine. Cannabis was the most consumed drug, with weekly consumption rates of 8575 mg –1 day –1 1000 inhabitants in community A and 16,978 mg –1 day –1 1000 inhabitants in community B, especially during the Carnival period. Methamphetamine was the least consumed, detected only during Carnival days, underscoring its recreational use. Additionally, stimulant drug use more than doubled during Carnival compared to the reference week, highlighting the significant impact of the festivities. The statistical analysis enabled distinguishing collection periods and highlighting key consumption trends. These findings provide valuable insights into drug use patterns and demonstrate the effectiveness of WBE for monitoring illicit drug consumption.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.002
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Methods · Consensus signal: none
Teacher disagreement score0.008
Threshold uncertainty score0.016

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.002
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0030.001
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.102
GPT teacher head0.453
Teacher spread0.351 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreMethods

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes1
Has abstractyes

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