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Record W4415482203 · doi:10.1039/d5sm00788g

A single molecule stimuli-robust fluorescent hydrogel based on excited state intramolecular proton transfer

2025· article· en· W4415482203 on OpenAlexafffund
Ankur A. Awasthi, Luís Teixeira Alves Duarte, Fabiano Severo Rodembusch, Teresa Dib Zambón Atvars, Cornelia Bohne

Bibliographic record

VenueSoft Matter · 2025
Typearticle
Languageen
FieldMaterials Science
TopicLuminescence and Fluorescent Materials
Canadian institutionsUniversity of Victoria
FundersNatural Sciences and Engineering Research Council of CanadaAmerican Chemical Society Petroleum Research FundInstituto Nacional de Ciência e Tecnologia em Eletrônica OrgânicaConselho Nacional de Desenvolvimento Científico e TecnológicoCoordenação de Aperfeiçoamento de Pessoal de Nível SuperiorFundação de Amparo à Pesquisa do Estado de São Paulo
KeywordsIntramolecular forceExcited stateFluorescenceMoleculeMicelleEmission spectrumSupramolecular chemistryProton

Abstract

fetched live from OpenAlex

'-bis(salicylidene)-(2-(3',4'-diaminophenyl)benzothiazole) (BTS) into a polyethylene oxide-polypropylene oxide-polyethylene oxide (PEO-PPO-PEO, F127) triblock copolymer hydrogel. BTS undergoes excited state intramolecular proton transfer (ESIPT), which leads to a broad emission spectrum where both the normal (N*) and tautomeric (T*) forms of the excited states of BTS coexist. Aggregation of BTS was prevented when it was embedded in F127 hydrogels. The BTS emission spectra are sensitive to the BTS loading in the gel, with white light being observed for some concentrations of lumiphore. In contrast, the BTS emission spectra are insensitive to pH. These experiments showed the successful application of a supramolecular strategy where the lumiphore is incorporated into a specific environment in the micelles forming the gel. The insensitivity of the emission colour to pH showed that emissive materials using a single ESIPT molecule can be achieved without the pH sensitivity normally associated with this process. These results highlight the importance of designing fluorophores with properties that enable them to be located in specific environments of supramolecular systems.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesInsufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.032
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.002

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.234
Teacher spread0.221 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes2
Has abstractyes

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