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Record W4415554312 · doi:10.1016/j.aca.2025.344698

DIATAGeR: Triacylglycerol annotation of data-independent acquisition based lipidomics

2025· article· en· W4415554312 on OpenAlexafffund
Linglan Zhu, Yong Jin Lim, Tao Huan, Thomas J. Velenosi

Bibliographic record

VenueAnalytica Chimica Acta · 2025
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicMetabolomics and Mass Spectrometry Studies
Canadian institutionsUniversity of British Columbia HospitalUniversity of British Columbia
FundersNational Cancer InstituteNatural Sciences and Engineering Research Council of CanadaNational Institutes of Health
KeywordsLipidomicsAnnotationIdentification (biology)Mass spectrometryMultiplexing

Abstract

fetched live from OpenAlex

BACKGROUND: Triacylglycerols (TGs) are the most abundant lipids in the human body and the primary source of energy storage. TGs are comprised of three fatty acyls with various lengths and double bond composition, complicating structural annotation when performing lipidomics by LCMS. Data-independent acquisition (DIA) based lipidomics enables a continuous and unbiased acquisition of all TGs, creating the potential for more comprehensive TG analysis. However, TG identification in DIA lipidomics data is challenging due to the difficulty analyzing multiplexed tandem mass spectra (MS2). RESULTS: In this study, we present DIATAGeR, an R package aimed to improve and automate TG identifications to the molecular species level in DIA-based lipidomics. With DIATAGeR, TGs are identified using a TG-centric approach, where each TG in the reference database is considered as an analysis target, searched in DIA spectra, and scored using a logistic regression machine learning algorithm. Additionally, DIATAGeR uses a false discovery rate (FDR) correction calculated by a target-decoy approach to improve the confidence of TG identification and limit false positives due to interference from unrelated ions. The performance of DIATAGeR was validated in a lipidomic study of liver and plasma samples from mice with metabolic dysfunction-associated steatohepatitis (MASH) and healthy controls. All 9 TG standards were annotated at an FDR <0.1 in both datasets. When benchmarked against MS-DIAL, TGs identified by DIATAGeR contained 18 % and 12 % more even-carbon fatty acyls in liver and plasma datasets, respectively. SIGNIFICANCE: DIATAGeR is a valuable tool for streamlining complex TG annotation in DIA-lipidomics data. It supports vendor-neutral MS spectra data formats and offers a customizable reference database. By combining TG-centric and target-decoy approaches, DIATAGeR showed improvements in TG identification by addressing primary challenges associated with multiplexed MS2 spectra. DIATAGeR is freely available at https://github.com/Velenosi-Lab/DIATAGeR.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.003
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.019
Threshold uncertainty score0.065

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0020.003
Meta-epidemiology (narrow)0.0030.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0020.001
Science and technology studies0.0010.001
Scholarly communication0.0020.002
Open science0.0020.002
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.0190.014

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.294
Teacher spread0.277 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations1
Published2025
Admission routes2
Has abstractno

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