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Record W4415647408 · doi:10.1002/cjce.70138

Green synthesis of nano‐crystallite <scp>CuO</scp> from waste sources for the enhancement of antimicrobial properties

2025· article· en· W4415647408 on OpenAlexvenueno aff
Md. Sahadat Hossain, Md. Ekhlas Uddin, Sumaya Tabassum, Sanjida Khan, Md. Najem Uddin, Samina Ahmed

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2025
Typearticle
Languageen
FieldMaterials Science
TopicCopper-based nanomaterials and applications
Canadian institutionsnot available
FundersBangladesh Council of Scientific and Industrial ResearchCouncil of Scientific and Industrial Research, India
KeywordsThermogravimetric analysisCrystalliteCrystallinityFourier transform infrared spectroscopyRietveld refinementPowder diffractionNanoparticleHydrothermal circulation

Abstract

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Abstract Global electronic waste has almost doubled since 2010, increasing from 33.8 MMT to over 62 MMT in 2022, and will reach 82 MMT by 2030. So, it will become the most pressing problem for the world if it cannot be utilized properly. In this research, Cu was collected from waste wire and used to synthesize CuO nanoparticles. The hydrothermal technique was properly employed, and X‐ray diffraction (XRD), thermogravimetric analysis (TGA), and Fourier transform infrared spectroscopy (FTIR) were used to characterize the prepared CuO nanoparticles. Scherrer's equation, linear straight‐line method, Monshi–Scherrer's method, size‐strain plot method, Williamson–Hall method, Sahadat–Scherrer's model, and Halder–Wagner method were applied to evaluate the crystallite size, preference growth, volume of the unit cell, lattice parameters, degree of crystallinity, macrostrain, energy density, and crystallinity index of the developed CuO samples. All models, except the linear straight‐line model, computed that crystallite size was within the acceptable range of 1–100 nm. The Rietveld refinement reported that the synthesized compound consisted of CuO phases and a small amount of Cu 2 O, which was negligible. The antimicrobial action of synthesized CuO nanoparticles was examined against gram‐negative ( Escherichia coli ) and gram‐positive ( Staphylococcus aureus ) bacteria. The investigations found that a significant inhibition zone was created for those microorganisms.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.421

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.187
Teacher spread0.177 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes1
Has abstractyes

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