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Record W4416031839 · doi:10.1016/j.wasman.2025.115229

Process optimization and techno-economic analysis of polyethylene terephthalate (PET) depolymerization in a non-aqueous alkaline environment for monomer recovery and reuse

2025· article· en· W4416031839 on OpenAlexafffund
Aakash Chakraborty, Damián J. Castillo-Preciado, Beza Moges, Zannat Mahal, Kang Kang, Arturo Sánchez, Sudip Kumar Rakshit

Bibliographic record

VenueWaste Management · 2025
Typearticle
Languageen
FieldMaterials Science
TopicPolymer crystallization and properties
Canadian institutionsLakehead University
FundersMitacsCanada Research Chairs
KeywordsDepolymerizationTerephthalic acidPolyethylene terephthalateResponse surface methodologySonicationMonomerProcess optimization

Abstract

fetched live from OpenAlex

This study presents a comprehensive investigation into optimizing polyethylene terephthalate (PET) depolymerization under alkaline conditions using response surface methodology (RSM). The critical process parameters studied were temperature, NaOH concentration, and reaction time. In the first phase, the combined effect of ozone pretreatment and ultrasound assistance on depolymerization efficiency was examined, revealing a positive direct correlation. In the second phase, RSM optimization with ozone pretreatment with ultrasonication conditions achieved 83.58% terephthalic acid (TPA) recovery and a total monomer recovery of 92.14%. Notably, applying the RSM-optimized conditions to virgin PET samples without pretreatment yielded comparable results thus highlighting the importance of statistical optimization tools. Techno-economic analysis using RSM optimized conditions for plant capacities ranging from 2.4 to 72 MT/day identified a minimum selling price of $1,533 USD/MT for TPA at the largest making it competitive with virgin TPA and other depolymerization methods. Sensitivity analysis highlighted feedstock and equipment costs as primary economic drivers, revealing opportunities for cost optimization.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: Simulation or modeling
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.156
Threshold uncertainty score0.447

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.222
Teacher spread0.217 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations4
Published2025
Admission routes2
Has abstractyes

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