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Record W4416086869 · doi:10.1016/j.seppur.2025.135998

Enhancing starch hydrolysate syrup purification: long-term ultrafiltration membrane performance under industrial conditions

2025· article· en· W4416086869 on OpenAlexaboutno aff
Camila Cabeza, Amal El Gohary Ahmed, Mario Minauf, Karin Wieland, Michael Harasek

Bibliographic record

VenueSeparation and Purification Technology · 2025
Typearticle
Languageen
FieldEnvironmental Science
TopicMembrane Separation Technologies
Canadian institutionsnot available
FundersÖsterreichische ForschungsförderungsgesellschaftTechnische Universität Wien BibliothekTechnische Universitat Wien
KeywordsUltrafiltration (renal)MembraneFoulingHydrolysateMembrane foulingStarchMembrane technologyBioprocess

Abstract

fetched live from OpenAlex

Ultrafiltration (UF) membranes based on Polyethersulfone (PES) are extensively used in food and bioprocessing industries for their good mechanical robustness and chemical resistance. In starch and sweetener production, these membranes play a vital role in clarifying and purifying carbohydrate-rich syrups. However, sustaining membrane performance under industrial conditions, characterised by elevated temperatures, high pressures, and chemically complex feed solutions, remains a significant challenge due to progressive fouling, membrane ageing, and irreversible performance decline. This study investigates the long-term performance (32h) of the GR90PP tight PES UF membrane (5 kDa cut-off) from Alfa Laval, operated under representative industrial conditions (60 °C, 8 bar) and using a real DE40 starch hydrolysate syrup. The study focuses on quantifying operational stability and fouling–cleaning behaviour across four filtration-cleaning cycles, including analysis of flux evolution, cleaning efficiency, solute rejection, and membrane integrity. Results revelaled a progressive Relative Flux Reduction (RFR), averaging 44 %, alongside a significant Flux Recovery Ratio (FRR) after cleaning, peaking at 80 % after the last alkaline rinse. Scanning Electron Microscopy (SEM) analysis confirmed a gradual build-up of fouling layer, predominantly organic in nature, contributing to reduced permeability and moderate irreversible fouling (average 21 %). Alkaline cleaning proved significantly more effective than acidic cleaning, highlighting the dominance of organic fouling mechanisms. Overall, the GR90PP membrane demonstrated strong operational stability, chemical compatibility, and cleaning resilience under extended high-temperature UF operation, supporting its suitability for processing of carbohydrate-rich products. These findings provide practical insights for optimising cleaning protocols, defining cleaning frequency, and adjusting operational parameters to sustain membrane performance in industrial food applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.289
Teacher spread0.267 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designObservational
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2025
Admission routes1
Has abstractyes

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