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Record W4416247275 · doi:10.1016/j.diamond.2025.113060

Spatial distribution of nitrogen and hydrogen in natural lithospheric diamonds by in situ synchrotron infrared microspectroscopy

2025· article· en· W4416247275 on OpenAlexfundno aff
Antonio Angellotti, Marta Morana, Lorenzo Barni, Gianfelice Cinque, Yongqiang Lu, Runzhe Tao, Giulia Marras, A. M. Logvinova, Luca Bindi, Д. С. Михайленко, Vincenzo Stagno

Bibliographic record

VenueDiamond and Related Materials · 2025
Typearticle
Languageen
FieldEarth and Planetary Sciences
TopicHigh-pressure geophysics and materials
Canadian institutionsnot available
FundersUral Branch, Russian Academy of SciencesSapienza Università di RomaChinese Academy of SciencesCanadian Anesthesiologists' SocietyDiamond Light Source
KeywordsChromiteSynchrotronDiamondHydrogenNitrogenChemical compositionInfraredAbsorption (acoustics)Analytical Chemistry (journal)Mineral

Abstract

fetched live from OpenAlex

Natural diamonds are exceptional carriers of mineralogical and chemical information from inaccessible depths of our planet. During their crystallization, they can host light elements such as H and N preserving a natural archive of mantle chemistry that, in turn, allows a better understanding of the chemical composition of the growth media, mechanisms of their formation and residence temperatures in the interior of Earth. However, how N and H distribute near entrapped minerals is still unknown. In this study we investigated the effect of chromite mineral inclusions on the spatial distribution of nitrogen and hydrogen in two natural diamonds of peridotitic origin using in situ synchrotron-based Fourier transform infrared microspectroscopy. From the acquisition and optimization of high-resolution maps, we determined the distribution of nitrogen, hydrogen, and nitrogen aggregation state. Our results reveal a dependence between the absorption of H-related peaks with the incorporation of pairs of nitrogen atoms ( N A-centers ). We explain it as indication that chemical interactions between chromite and H might be masked by variations in the N aggregation state. We also conclude that synchrotron micro-FTIR is an advanced technique to assist the synthesis of N- (and H-) doped diamonds for industrial applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.393
Threshold uncertainty score0.576

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.002
GPT teacher head0.183
Teacher spread0.181 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes1
Has abstractyes

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