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Record W4416529108 · doi:10.1016/j.cej.2025.170721

Citric acid - crosslinked cellulose derivatives superabsorbent hydrogels (SAH) as sustainable alternatives for personal hygiene applications

2025· article· en· W4416529108 on OpenAlexafffund
Muhammad Shahidul Islam, Dylan Sproule, Jessica Yohans, Pansit Chenananporn, Evelyn K. F. Yim, Arvind Gupta, Tizazu H. Mekonnen

Bibliographic record

VenueChemical Engineering Journal · 2025
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicHydrogels: synthesis, properties, applications
Canadian institutionsSurrey Memorial HospitalUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaMitacsCanada Research Chairs
KeywordsSelf-healing hydrogelsCarboxymethyl celluloseCelluloseBiocompatibilityBiodegradationBiopolymerCitric acidAbsorption of waterSwelling

Abstract

fetched live from OpenAlex

This study explores the development of citric acid (CA)-crosslinked superabsorbent hydrogels (SAHs) based on cellulose derivatives as sustainable alternatives to conventional petroleum-based superabsorbent polymers (SAPs) used in personal hygiene products. A biodegradable and biocompatible hydrogel formulation was synthesized using CA as a green crosslinking agent, with sodium carboxymethyl cellulose (Na-CMC) as the primary polymer and hydroxyethyl cellulose (HEC) as the secondary polymer, in varying ratios. The effects of polymer composition, swelling medium, pH, and water/saline solution absorption under load (AUL) were systematically evaluated by employing thermal analysis, rheology, water absorption capacity, swelling/deswelling kinetics, and soil biodegradation tests. Biocompatibility was also assessed via indirect contact cytotoxicity assays using mouse fibroblast cells. The optimized formulation, particularly the CMC—1.5 % CA hydrogel, exhibited high equilibrium water absorption (Q eq ) of 110 g/g in saline media at 38 °C, favorable swelling/deswelling behavior, rheological robustness, significant biodegradability (72 % within 7 weeks under composting conditions), and non-cytotoxicity (>80 % cell viability). These results highlight the potential of these hydrogels as biodegradable, biocompatible materials aligned with the Sustainable Development Goals (SDGs), especially for eco-friendly hygiene applications. • Citric acid–crosslinked cellulose hydrogels showed superior water absorption, exceeding commercial superabsorbents. • Hydrogels were up to 72 % biodegradable and non-cytotoxic, meeting key safety requirements. • Green-crosslinked cellulose hydrogels offer an eco-friendly alternative to synthetic absorbent materials. • The hydrogel process is simple, high-yield (>85 %), and scalable for industrial hygiene applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.367
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.243
Teacher spread0.235 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations11
Published2025
Admission routes2
Has abstractyes

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