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Record W4417005787 · doi:10.1021/acs.langmuir.5c04585

Why Doesn’t It Stick? Revealing the Impact of Mobile Oligomers on Ecoflex Surface Functionality and Bonding

2025· article· en· W4417005787 on OpenAlexafffund
Gloria M. D’Amaral, Hannah R. Jessop, Rahaf Nafez Hussein, Tricia Breen Carmichael

Bibliographic record

VenueLangmuir · 2025
Typearticle
Languageen
FieldEngineering
TopicAdvanced Sensor and Energy Harvesting Materials
Canadian institutionsUniversity of Windsor
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsPolydimethylsiloxaneElastomerWettingSiliconeAdhesionBiofoulingStretchable electronicsSurface modificationSiloxane

Abstract

fetched live from OpenAlex

Achieving stable interfacial performance in soft electronics requires a nuanced understanding of how the bulk elastomer composition affects surface functionality. This relationship is well-established in Sylgard 184, a polydimethylsiloxane (PDMS) elastomer that, upon oxidation, forms a cohesive SiO x surface supporting strong adhesion to vapor- and solution-deposited functional films. In contrast, Ecoflex, a widely used ultrasoft silicone elastomer, exhibits a long-recognized but poorly understood incompatibility with metal and solution-processed conductors. Here, we introduce layered PDMS/Ecoflex composites as a new experimental platform for systematically probing this limitation. We show that mobile low-molecular-weight siloxane oligomers in Ecoflex can migrate through a 100 μm thick PDMS membrane cross-linked directly to the Ecoflex substrate, significantly altering surface properties and undermining film deposition. By systematically removing and reintroducing these additives, we demonstrate their pivotal role in driving wetting failure, adhesion loss, and electrical degradation. While removing the additives enables the deposition of uniform, adherent, and conductive gold films, these species are also essential to Ecoflex’s extreme softness, revealing an inherent trade-off between surface functionality and mechanical compliance. Upon reintroduction, the oligomers restore softness but reverse the interfacial improvements, even compromising previously well-adhered films. These findings clarify the origin of Ecoflex’s surface instability and underscore the need to consider bulk formulation when designing elastomer interfaces for soft electronics.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.276
Teacher spread0.262 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes2
Has abstractyes

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