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Penikisite, BaMg<sub>2</sub>Al<sub>2</sub>(PO<sub>4</sub>)<sub>3</sub>(OH)<sub>3</sub>, isostructural with bjarebyite

2013· article· en· W5809008 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

aboutThe title or abstract carries a Canadian signal from the geographic lexicon.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueActa Crystallographica Section E Structure Reports Online · 2013
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsnot available
Fundersnot available
KeywordsTriclinic crystal systemCrystallographyIsostructuralOctahedronCrystal structureChemistryGroup (periodic table)BariumCrystal (programming language)Space groupX-ray crystallographyInorganic chemistryDiffractionPhysics

Abstract

fetched live from OpenAlex

The bjarebyite group of minerals, characterized by the general formula BaX(2)Y(2)(PO(4))(3)(OH)(3), with X = Mg, Fe(2+) or Mn(2+), and Y = Al or Fe(3+), includes five members: bjarebyite BaMn(2+) (2)Al(2)(PO(4))(3)(OH)(3), johntomaite BaFe(2+) (2)Fe(3+) (2)(PO(4))(3)(OH)(3), kulanite BaFe(2+) (2)Al(2)(PO(4))(3)(OH)(3), penikisite BaMg(2)Al(2)(PO(4))(3)(OH)(3), and perloffite BaMn(2+) (2)Fe(3+) (2)(PO(4))(3)(OH)(3). Thus far, the crystal structures of all minerals in the group, but penikisite, have been determined. The present study reports the first structure determination of penikisite (barium dimagnesium dialuminium triphosphate trihydroxide) using single-crystal X-ray diffraction data of a crystal from the type locality, Mayo Mining District, Yukon Territory, Canada. Penikisite is isotypic with other members of the bjarebyite group with space group P2(1)/m, rather than triclinic (P1 or P-1), as previously suggested. Its structure consists of edge-shared [AlO(3)(OH)(3)] octa-hedral dimers linking via corners to form chains along [010]. These chains are decorated with PO(4) tetra-hedra (one of which has site symmetry m) and connected along [100] via edge-shared [MgO(5)(OH)] octa-hedral dimers and eleven-coordinated Ba(2+) ions (site symmetry m), forming a complex three-dimensional network. O-H⋯O hydrogen bonding provides additional linkage between chains. Microprobe analysis of the crystal used for data collection indicated that Mn substitutes for Mg at the 1.5% (apfu) level.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies, Scholarly communication, Research integrity
Consensus categoriesMeta-epidemiology (narrow), Research integrity
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.088
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0040.003
Meta-epidemiology (broad)0.0040.002
Bibliometrics0.0020.004
Science and technology studies0.0030.002
Scholarly communication0.0020.004
Open science0.0020.001
Research integrity0.0030.004
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.204
Teacher spread0.198 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it