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Additional file 1 of Synthesis, characterization and antimicrobial properties of two derivatives of pyrrolidine-2,5-dione fused at positions-3,4 to a dibenzobarrelene backbone

2022· article· en· W6902170560 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueFigshare · 2022
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicSynthesis and Biological Activity
Canadian institutionsCarleton University
Fundersnot available
KeywordsProton NMRMass spectrumCarbon-13 NMRCompound semiconductorMass spectrometryNuclear magnetic resonance spectroscopyCharacterization (materials science)

Abstract

fetched live from OpenAlex

Additional file 1: Figure S1. UV Spectrum of compound 5. Figure S2. IR Spectrum of compound 5. Figure S3. Mass Spectrum of compound 5. Figure S4. 1H NMR of compound 5. Figure S5. COSY of compound 5. Figure S6. 13C NMR of compound 5. Figure S7. HSQCSpectrum of compound 5. Figure S8. HMBC Spectrum of compound 5. Figure S9. UV Spectrum of compound 8. Figure S10. IR Spectrum of compound 8. Figure S11. HRMS ESI-Positive mode of compound 8. Figure S12. Mass Spectrumfragmentation of compound 8. Figure S13. 1H NMR of compound 8. Figure S14. 13C NMR of compound 8. Table S1. ARRIVE Essential 10. Table S2. ARRIVE Recommended Set.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.584
Threshold uncertainty score0.417

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.5840.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.210
Teacher spread0.189 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it