Additional file 1 of Synthesis, characterization and antimicrobial properties of two derivatives of pyrrolidine-2,5-dione fused at positions-3,4 to a dibenzobarrelene backbone
Bibliographic record
Abstract
Additional file 1: Figure S1. UV Spectrum of compound 5. Figure S2. IR Spectrum of compound 5. Figure S3. Mass Spectrum of compound 5. Figure S4. 1H NMR of compound 5. Figure S5. COSY of compound 5. Figure S6. 13C NMR of compound 5. Figure S7. HSQCSpectrum of compound 5. Figure S8. HMBC Spectrum of compound 5. Figure S9. UV Spectrum of compound 8. Figure S10. IR Spectrum of compound 8. Figure S11. HRMS ESI-Positive mode of compound 8. Figure S12. Mass Spectrumfragmentation of compound 8. Figure S13. 1H NMR of compound 8. Figure S14. 13C NMR of compound 8. Table S1. ARRIVE Essential 10. Table S2. ARRIVE Recommended Set.
Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.
How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.002 | 0.012 |
| Meta-epidemiology (narrow) | 0.002 | 0.001 |
| Meta-epidemiology (broad) | 0.002 | 0.001 |
| Bibliometrics | 0.002 | 0.003 |
| Science and technology studies | 0.001 | 0.000 |
| Scholarly communication | 0.002 | 0.002 |
| Open science | 0.002 | 0.001 |
| Research integrity | 0.002 | 0.002 |
| Insufficient payload (model declined to judge) | 0.886 | 0.294 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".