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Dibenz[<i>b</i>,<i>f</i>]oxepin\nand Antimycobacterial Chalcone Constituents of <i>Empetrum nigrum</i>

2016· article· en· W6903039385 on OpenAlexaboutno aff

Bibliographic record

VenueFigshare · 2016
Typearticle
Languageen
FieldChemistry
TopicSynthesis and biological activity
Canadian institutionsnot available
Fundersnot available
KeywordsAntimycobacterialChalconeBiological activityFolk medicineNuclear magnetic resonance spectroscopy

Abstract

fetched live from OpenAlex

Two new dibenz­[<i>b</i>,<i>f</i>]­oxepins, empetroxepins A and B (<b>1</b> and <b>2</b>), and seven known compounds (<b>3</b>–<b>9</b>) were isolated from an extract of the Canadian medicinal\nplant <i>Empetrum nigrum</i> that significantly inhibited\nthe growth of <i>Mycobacterium tuberculosis</i> H37Ra. The\nstructures of <b>1</b> and <b>2</b> were established through\nanalysis of NMR and MS data. The antimycobacterial activity of the\nplant extract was attributed primarily to the presence of two chalcone\nderivatives (<b>6</b> and <b>7</b>) that exhibited selective\nantimycobacterial activity (IC<sub>50</sub> values of 23.8 and 32.8\nμM, respectively) in comparison to mammalian (HEK 293) cells\n(IC<sub>50</sub> values of 109 and 249 μM, respectively).

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.006
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.542
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.006
Meta-epidemiology (narrow)0.0020.002
Meta-epidemiology (broad)0.0030.002
Bibliometrics0.0000.001
Science and technology studies0.0010.001
Scholarly communication0.0000.001
Open science0.0030.002
Research integrity0.0020.001
Insufficient payload (model declined to judge)0.1820.005

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.028
GPT teacher head0.236
Teacher spread0.208 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2016
Admission routes1
Has abstractyes

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