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Record W6903145944 · doi:10.1021/op050014v.s003

Unification of Reaction Metrics for Green Chemistry II:  Evaluation of Named\nOrganic Reactions and Application to Reaction Discovery

2016· article· en· W6903145944 on OpenAlexaff

Bibliographic record

VenueFigshare · 2016
Typearticle
Languageen
FieldEnvironmental Science
TopicChemistry and Chemical Engineering
Canadian institutionsYork University
Fundersnot available
KeywordsContext (archaeology)Metric (unit)UnificationYield (engineering)Scope (computer science)Production (economics)Inverse

Abstract

fetched live from OpenAlex

The concept of minimum atom economy (AE)<sub>min</sub> and maximum\nenvironmental impact factor <i>E</i><sub>max</sub> is introduced and applied to\na database of more than 400 named organic reactions by\nemploying generalized Markush structures as a means of\ngauging worst-case scenarios for waste production for chemical\nreactions. The scope of the method can be extended to evaluate\n“green” performances for any chemical reaction once all\nbyproducts are identified. From the inverse relationship connecting AE and <i>E</i><sub>mw</sub> (environmental impact factor based on\nmolecular weight) and an analogous one connecting RME\n(reaction mass efficiency) and <i>E</i> (Sheldon environmental impact\nfactor), a minimum value of AE or RME equal to the golden\nratio, 0.618 (or 61.8%), is suggested as a threshold metric for\ngauging the true “greenness” of reactions. The rationale for\nthis is that this condition is met when the magnitude of AE\nexceeds that of <i>E</i><sub>mw</sub> and similarly when RME exceeds <i>E</i>.\nProbabilities for achieving this condition are also determined\nfor several organic reactions, and general expressions for\nevaluating such probabilities as functions of a general threshold\nα between 0 and 1 are also derived. Reactions in the database\nare classified according to general reaction types, and each class\nis ranked according to the “golden” threshold metric. Patterns\nwith respect to atom economical efficiency revealed by this\nanalysis are discussed, including the introduction of expressions\nfor determining the viability of recycling waste byproducts back\nto reagents. It is shown that the database can be used in a\ndiversity-oriented approach to discover new multicomponent\nreactions (MCRs) by combinatorial analysis of Markush fragments. In this context the top seven most frequently appearing\nMarkush structures in the database yield 33 viable three-component MCRs of which 12 have literature precedence.\nSynthetic strategies for reaction design are put forward using\nthe optimum criteria suggested by analysis of the database.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.017
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.247
Teacher spread0.226 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2016
Admission routes1
Has abstractyes

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