Influence of cooling rates on microstructure and mechanical performance of continuous fiber reinforced PPS composites
Bibliographic record
Abstract
In this study, the influence of the cooling rate on the crystallization temperature, level of crystallinity, spherulite size and mechanical properties was investigated for two continuous fibers reinforced polyphenylene sulfide (PPS) composites. Crystallization temperature and level of crystallinity were first studied by differential scanning calorimetry (DSC) for cooling rates comprised between 5 and 70°C/min. Results obtained showed that level of crystallinity was not significantly influenced by the cooling rate, while crystallization temperature decreased with increasing cooling rate. Matrix microstructure and composite short beam shear strength were then characterized for cooling rates of 3, 15 and 20°C/min. These cooling rates were chosen because they are representative of cooling rates used in autoclave manufacturing and compression molding. To enhance the microstructure of the PPS matrix, an etching solution based on potassium permanganate and orthophosphoric acid was used.
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How this classification was reachedexpand
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.002 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.005 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one teacher head, not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".