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Record W7007863601

ADSORPTION OF PHARMACEUTICALS FROM CONTAMINATED WATER BY ADSORBENTS DEVELOPED FROM REED CANARY GRASS

2023· dissertation· en· W7007863601 on OpenAlexfundno aff

Bibliographic record

VenueUniversity Library (University of Saskatchewan) · 2023
Typedissertation
Languageen
FieldEnvironmental Science
TopicAdsorption and biosorption for pollutant removal
Canadian institutionsnot available
FundersNatural Sciences and Engineering Research Council of CanadaUniversity of SaskatchewanCanadian Light Source
KeywordsAdsorptionActivated carbonWastewaterContaminationSurface waterEnvironmental remediationBiomass (ecology)Exothermic processHumic acid
DOInot available

Abstract

fetched live from OpenAlex

Discharge of pharmaceuticals into aquatic environments has been an emerging concern and removal of pharmaceuticals from water is very important. Sulfamethoxazole (SMX) is a frequently detected contaminant in wastewater and surface water and is a model of pharmaceutical contaminants because they have similar functional groups. Adsorption processes can be an effective technology to remove the pollutants. In this research, lignocellulosic material reed canary grass and activated carbons developed from this biomass were used as novel adsorbents to remove SMX. Surface area of the adsorbents played an important role in the adsorption process. The activated carbon with the highest surface area showed the highest adsorption capacity among the adsorbents. The SMX adsorption capacity favored acidic pH. Sips model simulated the experimental data well and was suitable since the adsorbent’s surface was heterogeneous. Existence of trimethoprim (TMP) in water affected SMX adsorption. Competitive adsorption of SMX and TMP decreased the adsorption capacity of the molecules compared to their single component adsorption. The change in enthalpy of SMX adsorption and activation energy were -45.5 and 35.2 kJ/mol, respectively, indicating the process was exothermic and primarily physisorption. Weighted mean of site energy distribution decreased from 11.21 kJ/mol at 15 °C and 11. 22 kJ/mol at 25 °C to 9.6 kJ/mol at 35 °C, showing stronger interactions at the lower temperature. π-π interactions, hydrogen bonding, Lewis acid base interactions, and hydrophobic interactions were the possible mechanisms that could be responsible for the adsorption. For the adsorbents with mean particle sizes of 84 and 216 μm, surface adsorption was rate controlling and the pseudo-second order model fitted the data better. For the adsorbent with larger particle size, diffusion was rate controlling and the pseudo-second order model simulated the data better. Desorbing the contaminant with methanol was more effective compared to aqueous solvents. The adsorbent could be reused for SMX adsorption during consecutive adsorption-desorption cycles. The adsorbents demonstrated capabilities to effectively adsorb SMX and showed a potential to remove SMX and similar pharmaceutical pollutants from real contaminated water.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.001
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.194
Teacher spread0.184 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2023
Admission routes1
Has abstractyes

Explore more

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