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Record W7008025390

Applications of Graphene in Vanadium Redox Flow Batteries

2023· dissertation· en· W7008025390 on OpenAlexfundno aff

Bibliographic record

VenueUWSpace (University of Waterloo) · 2023
Typedissertation
Languageen
FieldEngineering
TopicAdvanced battery technologies research
Canadian institutionsnot available
FundersAlberta Innovates
KeywordsFlow batteryGrapheneNafionVanadiumRedoxMembraneOxideElectrode
DOInot available

Abstract

fetched live from OpenAlex

Vanadium redox flow batteries (VRFBs) exhibit great promise as easily scalable, long-lasting, modular systems for grid-scale energy storage. However, vanadium crossover and poor reaction kinetics increase their operating costs by requiring frequent system regeneration and reducing energy efficiency, respectively. In this thesis, Nafion membranes were modified with single to few-layer nitrogen/sulfur-doped graphene (NS-graphene) by developing a large area Langmuir film deposition method with the aim of reducing vanadium crossover and potentially improving reaction kinetics. Using this approach, the ability to reduce vanadium permeability through Nafion 117 and Nafion 115 membranes by 75% and 53%, respectively, was demonstrated while maintaining a high enough proton conductivity that the overall selectivity of the membranes was increased by 243% and 65% when compared to the results for bare Nafion. To determine the impact of the intrinsic electrocatalytic activity of graphene on redox flow battery performance, a comparison of NS-graphene, graphene oxide (GO), and reduced graphene oxide (RGO) was carried out using both monolayer electrodes and drop-cast films. Through this work, it was confirmed that the previously established approach developed by Punckt et al. [1] to account for porosity could not be extended to quasi-reversible systems such as that of the VRFB. An alternative data analysis scheme based on Dunn’s Method is proposed, showing mildly promising results, with more work needed in the area to develop strong conclusions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Qualitative · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.545
Threshold uncertainty score0.936

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.214
Teacher spread0.206 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designQualitative
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2023
Admission routes1
Has abstractyes

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