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Record W7026791247

Atomistic study of magnetite thin film interfaces and defects for Spintronic applications
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2015· dissertation· en· W7026791247 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueWhite Rose eTheses Online (University of Leeds, The University of Sheffield, University of York) · 2015
Typedissertation
Languageen
FieldMaterials Science
TopicMagnetic Properties and Synthesis of Ferrites
Canadian institutionsYork University
Fundersnot available
KeywordsWork (physics)PermalloySubstrate (aquarium)Ferromagnetism
DOInot available

Abstract

fetched live from OpenAlex

Fe3O4 is a candidate material for future spintronic device applications due to its predicted half metallicity, high Curie temperature and lattice match with current oxide barrier materials. There have been numerous studies on Fe3O4(001)/MgO(001) heterostructures and devices in recent years which show structural defect formation has a significant influence on the properties of the grown layers and device performance. In this work I seek to advance our understanding of defect formation and heterostructure interfaces of epitaxially grown Fe3O4 layers on a range of substrates. Atomically resolved (S)TEM/EELS has been used as a main experimental techniques to determine the atomic structure of the defects and interfaces in order to model their effect of the functional properties of the thin films magnetite. 
\nFirstly we investigate the MBE growth of (111) oriented Fe3O4/MgO thin films. This creates highly ordered, atomically sharp APB defect boundaries rather than the random-like fractal geometry defects which have previously been observed in (001) oriented growth. This has enabled us to undertake atomistic modelling and begin to understand the APBs effect on the magnetic properties of grown films. We show that all APB defects exhibit a high density of high angle Fe-O-Fe bonds with antiferromagnetic coupling.
\n The Fe3O4/MgO structure produces a high density of APB defects, and consequently anomalous properties of the grown films such as negative magnetoresistance and high saturating magnetic fields. In order to avoid crystal symmetry as an origin of APBs we undertook a MBE growth of Fe3O4/MgAl2O4 a spinel-spinel growth system. However, the presence of the APBs was still observed and their formation was discussed in terms of strain and 3D film growth. 
\nTo reduce the density of defects in Fe3O4 we employed pulsed laser deposition with subsequent film annealing in a CO/CO2 atmosphere. This is shown to produce films with bulk like transport properties after a high temperature annealing process. Residual defects including twins were observed. These defects have a low density and the effect on overall film properties is small. 
\nFinally, using the spinel/perovskite model structure of Fe3O4/SrTiO3 we show the ability to produce atomically sharp oxide/oxide interfaces which open up the possibility of performing atomic level engineering to tailor potential oxide-oxide device functionality. 
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Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Qualitative · Consensus signal: Qualitative
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.336
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0020.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.222
Teacher spread0.203 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it