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Comparison of laser-induced breakdown spectroscopy, colour sensing, as well as visible, near-infrared, and mid-infrared spectroscopy to predict soil properties

2025· article· en· W7111057078 on OpenAlexafffundabout

Bibliographic record

VenueGeoderma · 2025
Typearticle
Languageen
FieldEngineering
TopicLaser-induced spectroscopy and plasma
Canadian institutionsCanada Malting (Canada)BGC Engineering (Canada)McGill UniversityInstitut National de la Recherche ScientifiqueEnvironment and Climate Change Canada
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsPartial least squares regressionMean squared errorCoefficient of determinationSoil testLinear regressionCation-exchange capacityAnalytical Chemistry (journal)Soil waterSpectroscopySoil organic matter

Abstract

fetched live from OpenAlex

• Seven different instruments to predict soil properties using the same samples were compared. • Soil properties included P, K, Ca, Mg, Al, buffer pH, pH, SOM, and CEC. • LIBS and Vis-NIR sensor systems produced results with relatively lower uncertainties. • Several prediction models, all for CEC, yielded relatively accurate predictions. • Neither instrument was able to overperform commercial labs for P, pH, Mg, and SOM. Seven spectroscopic instruments’ ability to predict nine soil chemical properties [ i.e. , extractable phosphorus (P), extractable potassium (K), calcium (Ca), magnesium (Mg), aluminum (Al), soil pH (pH), buffer pH (BpH), soil organic matter (SOM) and cation exchange capacity (CEC)] were assessed using a diverse set of 798 air-dried and compressed soil samples from Southern Quebec. The instruments varied in terms of spectral range and resolution [ e.g ., colour/visible (Vis), visible and near-infrared (Vis-NIR), mid-infrared (MIR), and laser-induced breakdown spectroscopy (LIBS)], complexity, and interaction with the target. The performance of these instruments was compared using relevant test statistics derived from partial least squares regression (PLSR) models, such as the root mean squared error of prediction (RMSE P ) and the coefficient of determination (R 2 ) for simple linear regressions between sensor measurements and soil test reference values. Analysis of the LIBS spectra produced the lowest RMSE P values for P, K, Mg, Ca, pH, BpH, and SOM, while two Vis-NIR instruments yielded prediction models with the lowest RMSE P for Al and CEC. Overall, prediction models were relatively accurate for Ca, Mg, Al, SOM, and CEC (R 2 = 0.70–0.81), and less certain for P, pH, BpH, and K (R 2 = 0.53–0.65).

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.085
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.260
Teacher spread0.249 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2025
Admission routes3
Has abstractyes

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