From Kraft Pulp Fibers to Si-O-C Ceramics via Sol-Gel Synthesis: Impact of Functionalization and Pre-Pyrolysis
Bibliographic record
Abstract
This study investigated the fabrication of C/SiO₂ ceramics using kraft pulp fibers (KF) and phosphorylated kraft pulp fibers (PKF) impregnated with a ceramic precursor via a sol-gel route. The rheological behaviour coupled to infrared spectroscopy of the ceramic precursor was examined to optimize the drying process of the impregnated preforms. Thermo-gravimetric analysis and scanning electron microscopy were used to study the thermal behaviour and micro-structure of the ceramics. The PKF exhibited a superior thermal stability, and enhanced fiber/ceramic interactions compared to untreated KF. The impact of the fiber functionalization and of the pre-pyrolysis of PKF on fiber/ceramic interactions was also explored. The in-situ formation of carbon fibers during heat treatment from PKF appears to be a more effective approach for developing future environmentally sustainable ceramic matrix composites (CMCs).
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How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.001 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".