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Record W7132899107

Percolation and Adsorption of Volatile Organic Compounds onto Hyper Activated Renewable Carbon for Low-carbon Composites Manufacturing

2024· dissertation· W7132899107 on OpenAlexafffund
Bo Sun

Bibliographic record

VenueTSpace · 2024
Typedissertation
Language
FieldEnvironmental Science
TopicAdsorption and biosorption for pollutant removal
Canadian institutionsUniversity of Toronto
FundersNatural Sciences and Engineering Research Council of CanadaFord Motor Company
KeywordsAdsorptionActivated carbonKineticsScanning electron microscopeFourier transform infrared spectroscopyRenewable energyPollutant
DOInot available

Abstract

fetched live from OpenAlex

Low-carbon composites (LCCs), as a type of biodegradable material consisting of lignocellulosic fibers and polymers, are considered as promising alternatives for petroleum derived plastics. However, the elimination of volatile organic compounds (VOCs) during the compounding of LCCs has been a long-struggled issue. These VOCs are highly toxic pollutants and carcinogens with strong odor, which have significantly limited the applications of LCCs in interior environments. Seeking an efficient adsorbent to capture the VOCs as well as systematically profiling its adsorption kinetics remains a challenge. In this study, we for the first time developed an innovative hyper activated renewable carbon (HARC), which possesses dominant alkaline groups of 0.133 mmol/g, large Brunauer-Emmett-Teller (BET) surface area of 1128.6 m2/g, as well as high adsorption energy of 25.24 kJ/mol. Its adsorption kinetics towards VOCs was further investigated to maximize the removal efficiency of VOCs. For this purpose, three different micrometer-sized HARC samples were prepared by alkali (NaOH) modification of renewable carbon, named as small sized HARC (S-HARC), medium sized HARC (M-HARC) and large sized HARC (L-HARC), respectively. Among these three samples, S-HARC exhibited the highest activity in capturing VOCs. Its fast migration velocity and better distribution inside the LCCs domain was demonstrated via dynamic simulation, which is advantageous in increasing its contact opportunities with VOCs molecules and favoring their adsorption. Scanning electron microscopy (SEM) revealed the different morphological structure of three HARC samples, and the concentration of surface groups was determined by Boehm titration. More than 120 compounds were identified via gas chromatography-mass spectroscopy (GC/MS), and the adsorption kinetics were analyzed based on the quantified VOCs content from mass spectroscopy (MS). The obtained adsorption data was better fitted in the linear form of Freundlich isotherms, rather than Langmuir isotherms. Compared with physical properties, the adsorption capacity of HARC was more correlated to the change in its chemical functionalities, especially the total alkaline groups. The finding in this study provides important information for deeper understanding of the adsorption and percolation dynamics of VOCs onto porous HARC. Using HARC, especially S-HARC, can significantly promote the removal of odorous VOCs, and open up new horizons of using LCCs as substitutes for traditional high-carbon plastics in broader industries.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.261
Teacher spread0.250 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2024
Admission routes2
Has abstractyes

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