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Record W7132933155

Developing Techniques for UV-visible Spectroscopy of Single Acoustically Levitated Aqueous Droplets for Applications in Atmospheric Chemistry

2024· dissertation· W7132933155 on OpenAlexaff
Christopher Boguslaw Rusiewicz

Bibliographic record

VenueTSpace · 2024
Typedissertation
Language
FieldEngineering
TopicMicrofluidic and Bio-sensing Technologies
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsAbsorbanceSpectroscopyAtmospheric pressureAtmospheric chemistryAqueous solutionAnalytical Chemistry (journal)
DOInot available

Abstract

fetched live from OpenAlex

Few studies have utilized UV-visible direct absorbance spectroscopy to probe acoustically levitated droplets, leading to a dearth of detailed procedures. Acoustically suspended droplets are an ideal contactless reaction compartment for investigating heterogeneous atmospheric chemistry. This is due to levitated droplets sharing similar properties to atmospheric droplets, such as high surface-area-to-volume-ratios. In this thesis, I describe a new apparatus and methodologies I developed to precisely control droplet evaporation, relative humidity, and atmospheric composition. The newly developed apparatus was used to investigate possible Brown Carbon (BrC) chemistry involving humic acid sodium salt, catechol, and water-soluble pine wood smoke extract, under variable atmospheres and illumination conditions. Results showed some deviation from bulk experiments, which may be attributed to pH changes inside levitated droplets, photochemical reactions, volatilization, and increased scattering. These results demonstrate that UV-visible direct absorbance spectroscopy of acoustically levitated droplets can be a powerful tool for studying atmospheric reactions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.002
Threshold uncertainty score0.008

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.001
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.0020.002

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.308
Teacher spread0.291 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2024
Admission routes1
Has abstractyes

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