SMA/Py/ZnO as a new biocompatible polymer supported nanocatalyst for the synthesis of chromeno[2,3-d] pyrimidine-diones through a novel and efficient pathway
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Bibliographic record
Abstract
An efficient and simple method for the synthesis of chromeno[2,3-d]pyrimidine-diones using SMA/Py/ZnO catalyst has been reported. Zinc oxide nanoparticles were coordinated on a modified poly(styrene-comaleic anhydride) (SMA) support to prevent agglomeration and reduction catalytic activity. The polymer support was easily prepared from the reaction of 3-aminopyridine with SMA. The catalyst was characterized by using various characterization techniques such as FTIR,1H NMR, SEM, and EDX. The catalytic activity of SMA/Py/ZnO for the synthesis of chromeno[2,3-d]pyrimidine-diones through a multicom-ponent reaction of 6-amino-1,3-dimethyl uracil, 3,4-methylenedioxyphenol, and an appropriate aryl aldehyde under solvent-free conditions was also studied. © 2019, Canadian Science Publishing. All rights reserved.
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Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.001 |
| Meta-epidemiology (narrow) | 0.001 | 0.001 |
| Meta-epidemiology (broad) | 0.002 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.001 | 0.001 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.002 | 0.001 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.005 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it