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Record W7165485872 · doi:10.82308/56025

Spatio-temporal metabolomic analysis of Lespedeza capitata

2025· dissertation· en· W7165485872 on OpenAlex
Puneet Kaur

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

aboutThe title or abstract carries a Canadian signal from the geographic lexicon.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

Venuenot available
Typedissertation
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicBioactive natural compounds
Canadian institutionsnot available
Fundersnot available
KeywordsFabaceaeLespedezaDaidzeinIsoflavonesMetabolomicsPhytochemistryNative plant

Abstract

fetched live from OpenAlex

Isoflavonoids are a class of plant specialized metabolites that are almost exclusively found in the Fabaceae (legume) family. These compounds play crucial roles in plant physiology, including facilitating symbiosis with nitrogen-fixing bacteria known as Rhizobia and protecting against pathogenic microbes. However, the occurrence and composition of the isoflavonoids and their derivatives are varied among the Fabaceae. There is a great array of structural diversity, especially in the chemical tailoring of the scaffold beyond the canonical isoflavones (e.g., daidzein and genistein). Correspondingly, there are lineage-specific divergences in the modes of biosynthesis, accumulation, and storage. The Lespedeza genus within the Fabaceae is underexplored except for initial profiling over two decades ago. Surprisingly, those early studies showcased the incredible diversity of isoflavonoids in the genus and indicated strong antioxidant and therapeutic potential. Thereafter, certain isoflavonoids derived from the Lespedeza spp., including phenoxodiol, have been identified as putative anticancer drug targets. However, there remains a dearth of metabolomic or genomic datasets to investigate the biosynthesis of this unique chemical repertoire. Lespedeza capitata Michx. is a noteworthy species within this genus, with agro-ecological and ethnobotanical relevance. Known commonly as roundheaded bushclover, it is native to the northeastern regions of the US and eastern Canada. This species has been the source of Indigenous medicines, including as a counter-irritant for rheumatism, analgesic for neuralgia, and antidote for poison. Several reports have showcased the pharmacotherapeutic properties of the plant extracts of L. capitata, including promoting healthy kidney functioning, tissue regeneration, and blood pressure regulation. However, there is a knowledge gap in understanding the bioactive compounds and their biosynthesis. Therefore, my thesis describes an in-depth spatio-temporal metabolomic profiling of L. capitata to capture the composition and content of isoflavonoids in several tissue and development stages. For a multi-omics approach, the harvested tissues were homogenized and divided into two parts for metabolite analysis, detailed here, and for RNA sequencing and transcriptomic analysis at a later date. Chemical analyses were performed using targeted and untargeted approaches with liquid chromatography triple-quadrupole mass spectrometry (LC/TQ-MS) and quadrupole time-of-flight mass spectrometry (LC/QTOF-MS) to quantify known metabolites and identify novel targets. Six known isoflavonoids were detected and quantified, including the isoflavone aglycones genistein and glycitein, their glycosylated counterparts genistin and glycitin, and the O-methylated isoflavonoids formononetin and biochanin A. In parallel, untargeted analysis was conducted, coupled with MS/MS collision-induced fragmentation of unknown peaks, providing predicted structures of twenty-three uncharacterized features belonging to the flavonoid and isoflavonoid classes. An interesting example is the pterocarpan “1-methoxyerythrabyssin II,” which was putatively identified and found most abundantly in mature roots. This isoflavonoid derivative has previously been reported in the related species L. bicolor and has been associated with inhibiting bacterial neuraminidase, a key enzyme in bacterial pathogenesis. To complement this detailed metabolomic profile, a list of legume-specific isoflavonoid gene targets has been curated that will allow the future querying of corresponding transcriptomic datasets. This spatio-temporal study of isoflavonoid metabolism in L. capitata creates a springboard for pathway discovery leading to high-value metabolites, including those with pharmacotherapeutic properties.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.064
Threshold uncertainty score0.924

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.289
Teacher spread0.278 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

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Citations0
Published2025
Admission routes1
Has abstractyes

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