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Peroxidation and redox reactions catalyzed by truncated hemoglobins

2015· article· en· W1462703244 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueThe FASEB Journal · 2015
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicHemoglobin structure and function
Canadian institutionsUniversité Laval
Fundersnot available
KeywordsHemeChemistryParacoccus denitrificansHistidinePeroxidaseStereochemistryFerricHemeproteinCofactorNitrite reductaseBiochemistryEnzymeInorganic chemistry

Abstract

fetched live from OpenAlex

Roseobacter denitrificans is one member of widespread marine Rosoebacters and performs photosynthesis and denitrification aerobically. We report a native heme‐bound R. denitrificans truncated hemoglobin ( Rd . trHb) from heterologous expression in E. coli . Rd . trHb exhibits absorbance at 412, 538 and 572 nm bands with predominately alpha‐helical secondary structure. The phylogenetic classification suggests that Rd . trHb falls into group II trHbs, whereas sequence alignments indicate that it shares important heme pocket residues with both groups I and II trHbs. The resonance Raman spectra indicate that ferric Rd . trHb is mostly 6‐coordinate low‐spin and the ferrous form is a mixture of 5‐ and 6‐coordinated states. Two Fe‐His stretching modes were detected: one at 228 cm ‐1 , which represents an unconstrained neutral histidine as in other trHbs, and the other at 248 cm ‐1 , which has been reported in peroxidases and some flavohemoglobins that contain Fe‐His‐Asp (or Glu) catalytic triad, but not in trHbs. Further, Rd . trHb exhibits a significant peroxidase activity with a ( k cat / K m ) value three orders of magnitude higher than bovine Hb and only one order lower than horseradish peroxidase (HRP). The pH‐rate profiles yield a pK a value ~6.8. Homology modeling suggests that residues known to be important for interactions with heme‐bound ligands in group II trHbs from M. tuberculosis and B. subtilis are pointing toward to heme in Rd . trHb. Genomic organization and gene expression profiles imply possible functions for detoxification of reactive oxygen and nitrogen species in vivo . Altogether, Rd . trHb exhibits some distinct features and appears equipped to help Roseobacters to cope with reactive oxygen/nitrogen species and/or operate redox biochemistry.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.074
Threshold uncertainty score0.233

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.235
Teacher spread0.223 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it