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Record W193916140 · doi:10.1096/fasebj.20.5.lb59

Closing the lid on the mono‐ADP‐ribosylating reaction mechanism by bacterial toxins

2006· article· en· W193916140 on OpenAlexaff
René Jørgensen, Xu Wang, Xiaobo Liu, Rod Merrill

Bibliographic record

VenueThe FASEB Journal · 2006
Typearticle
Languageen
FieldImmunology and Microbiology
TopicToxin Mechanisms and Immunotoxins
Canadian institutionsUniversity of Guelph
Fundersnot available
KeywordsActive siteChemistryConformational changeADP-ribosylationStereochemistryNAD+ kinaseCatalytic cycleTransferaseNucleotideBiochemistryEnzyme

Abstract

fetched live from OpenAlex

The bacteria causing diphtheria, whooping cough, cholera and other human diseases secrete mono‐ADP‐ribosylating toxins that modify intracellular proteins in the target host eukaryotic cell. Recently, we solved four crystal structures of a catalytically active complex between the enzyme domain of Exotoxin A (ETA) and its protein substrate, elongation factor 2 (eEF2), which has led to a breakthrough in the understanding of the reaction mechanism of this family of deadly toxins. The target residue in eEF2, a modified histidine called diphthamide, spans across a cleft in the complex and faces the two phosphates of the NAD + analogue, βTAD. This suggests that the diphthamide is involved in triggering NAD + cleavage and is interacting with the proposed oxacarbenium intermediate during the nucleophilic substitution reaction. Notably, the βTAD phosphates mimic the phosphate backbone of two nucleotides in a conformational switch of 18S rRNA, thereby achieving universal recognition of eEF2 by ETA. However, the structures do not reveal the transition state for the transferase reaction within the complex. We have new data showing that there are catalytic residues located within an active‐site loop of the toxin. We propose that this loop is in an open conformation in the protein complex structures and during transition‐state formation closes in on the active site partly as a cover for solvents and partly to help stabilize the oxacarbenium ion.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesScience and technology studies
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.012
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0020.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.211
Teacher spread0.199 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2006
Admission routes1
Has abstractyes

Explore more

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