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Record W1958551378 · doi:10.1002/mren.201200078

Analysis of Slurry‐<scp>P</scp>hase Co‐<scp>P</scp>olymerization of Ethylene and 1‐<scp>B</scp>utene by Ziegler–<scp>N</scp>atta Catalysts Part 1: Experimental Activity Profiles

2013· article· en· W1958551378 on OpenAlexaff
John T. McCoy, João B. P. Soares, Randhir Rawatlal

Bibliographic record

VenueMacromolecular Reaction Engineering · 2013
Typearticle
Languageen
FieldChemistry
TopicOrganometallic Complex Synthesis and Catalysis
Canadian institutionsUniversity of Waterloo
Fundersnot available
KeywordsNattaPolymerizationCatalysisReaction rate constantZiegler–Natta catalystKinetic energySlurryThermodynamicsChemistryPhase (matter)EthyleneMaterials sciencePolymer chemistryChemical engineeringKineticsPolymerOrganic chemistryComposite materialPhysics

Abstract

fetched live from OpenAlex

Abstract A rigorous method is developed to extract kinetic parameters describing catalyst activity from experimental polymerization rate profiles for Ziegler–Natta catalysts. The kinetic scheme used correlates the oxidation state with catalyst activity, eliminating the need for multiple site types to describe rate profiles. The method is applied to data from kinetic experiments performed in a lab‐scale semi‐batch reactor. Four parameters are required to describe the activity of the catalyst: the polymerization rate constant and three site transformation rate constants. The model is able to reproduce changes in the rate profiles in response to reactant concentrations. The fits of the model to the data are comparable to those in similar studies.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.002
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.028
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.002
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0010.002
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.215
Teacher spread0.207 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2013
Admission routes1
Has abstractyes

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