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Record W1963951456 · doi:10.1021/jp8089159

Volumetric Properties of Solvation in Binary Solvents

2009· article· en· W1963951456 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueThe Journal of Physical Chemistry B · 2009
Typearticle
Languageen
FieldChemical Engineering
TopicThermodynamic properties of mixtures
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsSolvationPartial molar propertyChemistrySolventThermodynamicsWork (physics)Aqueous solutionPhysical chemistryOrganic chemistryPhysics

Abstract

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The volumetric properties of solutes, including partial molar volume, compressibility, and expansibility, are determined by and, therefore, sensitive to the entire spectrum of solute-solvent interactions. However, applications of volumetric measurements to the study of solvation of solutes in binary solvents consisting of the principal solvent and a cosolvent are almost nonexistent. This deficiency partially reflects the lack of an adequate theoretical framework to rationalize the measured volumetric observables in terms of solute-principal solvent and solute-cosolvent interactions. To address this deficiency, we present in this work a simple statistical thermodynamic model describing solute thermodynamics in binary solvents. Based on the model, we derive relationships that link the partial molar volumetric properties of solutes with the extent and intensity of interactions of a solute with the principal solvent and the cosolvent. If the approximation of homogeneous solvation is introduced, the derived formalism can be simplified to a form that can be readily employed for practical treatment of experimental volumetric data on small solutes and/or individual atomic groups. As an example, we use this simplified formalism to rationalize the volumetric properties of the zwitterionic amino acid glycine in concentrated urea solutions. In general, the theoretical development presented in this work opens the way for systematic applications of volumetric measurements to quantitative characterization of solute-solvent interactions in complex solvents.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.027
Threshold uncertainty score0.258

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.212
Teacher spread0.201 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it