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Record W1972069759 · doi:10.1139/p02-140

Inelastic neutron scattering and low-energy excitation of amorphous SF<sub>6</sub> hydrate prepared by vapor-deposition technique

2003· article· en· W1972069759 on OpenAlexvenueno aff
Osamu Yamamuro, T. Matsuo, Itaru Tsukushi, Noriko Onoda‐Yamamuro

Bibliographic record

VenueCanadian Journal of Physics · 2003
Typearticle
Languageen
FieldEnvironmental Science
TopicMethane Hydrates and Related Phenomena
Canadian institutionsnot available
FundersHigh Energy Accelerator Research Organization
KeywordsAmorphous solidHydrateAnalytical Chemistry (journal)DopantInelastic neutron scatteringDopingNeutron scatteringHydrogenScatteringMaterials scienceCrystallographyPhysicsChemistryOpticsOrganic chemistry

Abstract

fetched live from OpenAlex

Amorphous SF6 hydrate (SF6·17H2O) was prepared by depositing the mixed vapor onto a substrate kept at about 8 K. The inelastic neutron-scattering spectra of the as-deposited sample and those annealed at about 120 and 150 K were measured at 50 K in the energy range below 100 meV. The first two samples were considered to be in amorphous states while the third one was in a crystalline state. The librational frequency of the water molecule (at around 60 meV) is smaller in the order of (as-deposited sample) < (annealed sample) < (crystalline sample). This indicates that the strength of the intermolecular hydrogen bonds is (crystalline sample) > (annealed sample) > (as-deposited sample). The spectra below 10 meV were compared with our previous data of pure vapor-deposited amorphous ices and those doped with methanol (CD3OH). The low-energy excitation (E < 6 meV) differed drastically depending on the dopants, i.e., the scattering intensity was enhanced by methanol doping but reduced by SF6 doping. This may be because the hydrogen-bond formation was hindered by methanol doping but promoted rather more by SF6 doping because of the hydrophobic interaction as in clathrate hydrates. PACS Nos.: 61.12Ex, 63.50tx

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.172
Teacher spread0.167 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2003
Admission routes1
Has abstractyes

Explore more

Same venueCanadian Journal of Physics→Same topicMethane Hydrates and Related Phenomena→French-language works237,207→