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Effects of Metal Ions on H2 Generation during Photolysis of Suspended TiO2 in Aqueous Systems

2015· article· en· W1984073080 on OpenAlex
G.R. Dey

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

venuePublished in a venue whose home country is Canada.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueJournal of Applied Solution Chemistry and Modeling · 2015
Typearticle
Languageen
FieldEnergy
TopicAdvanced Photocatalysis Techniques
Canadian institutionsnot available
FundersBhabha Atomic Research CentreDepartment of Atomic Energy, Government of India
KeywordsPhotocatalysisFormic acidChemistryScavengerAqueous solutionCatalysisPhotodissociationMetal ions in aqueous solutionCopperMetalContext (archaeology)Inorganic chemistryIonNanoparticleNoble metalPhotochemistryRadicalNanotechnologyMaterials scienceOrganic chemistry

Abstract

fetched live from OpenAlex

Nowadays, photocatalysis is being applied as a promising technique for decontamination, purification, deodorization, etc. of polluted air and wastewaters. This technique attempts also to generate renewable and non-polluting fuels utilizing various carbon and hydrogen sources. In this context, studies on photo-catalytic generation of H2 using 0.1% w/v TiO2 photo catalyst as a suspension in water was carried out using 350 nm light. This was explored further in presence of various metal ions such as Ag+, Cu2+, Fe2+, Au3+ and V5+ at different ambient such as air and CO2, in presence of a hole scavenger (2-propanol and formic acid). H2 yields in CO2-purged systems as analyzed in GC-TCD were reasonably higher, and increased further when metal ions were added into the systems. Based on H2 yields, HCOOH was found to be a more supportive hole scavenger as compared to 2-propanol in metal ions containing systems. Besides the formation of low to high concentrations of various gaseous products, nanoparticles of gold, silver and copper were also observed as photolysis products. This indicated that the presence of both reduced metal ions and their in-situ generated nanoparticles at various stages either in the free/unbound and/or associated with TiO2 photocatalyst in aqueous systems, together play a significant role in enhancing the H2 yields.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.152
Threshold uncertainty score0.455

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.026
GPT teacher head0.266
Teacher spread0.239 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it