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Investigation on the Synthesize Reaction Possibility of M(CO)<sub>2</sub>CY-Ph<sub>3</sub>XR(M=Cr, Mn; X=Sn, Ge; Y=S, Se; R= N(C<sub>4</sub>H<sub>4</sub>), N(C<sub>8</sub>H<sub>6</sub>), C<sub>6</sub>H<sub>5</sub>)

2011· article· en· W1984414885 on OpenAlexaff
Zheng Ping Wu, Ian S. Butler

Bibliographic record

VenueAdvanced materials research · 2011
Typearticle
Languageen
FieldEngineering
TopicMolecular Junctions and Nanostructures
Canadian institutionsMcGill University
Fundersnot available
KeywordsMetalLigand (biochemistry)Mulliken population analysisChemistryBenzeneCrystallographyPhysical chemistryStereochemistryComputational chemistryDensity functional theoryOrganic chemistry

Abstract

fetched live from OpenAlex

The thermodynamics properties of synthesize reactions of Ph3SnR (R= N (C4H4), N(C8H6), C6H5) and CpM(CO)2CY(M=Cr, Mn; Y=S, Se), the total energy and Mulliken atomic charges of the compound products M(CO)2CY-Ph3XR(M=Cr, Mn; X=Sn, Ge; Y=S, Se; R= N(C4H4), N(C8H6), C6H5) with different substitute positions on the benzene ring were investigated using DFT method. The calculation results of total energy showed that the ligand was determinant of the favourable substituted position and the central metal of two different type ligands CpCr(CO)2CY(Y=S, Se) and CpMn(CO)2 CY(Y=S, Se) was the key factor; whether the reactants Ph3SnR( R= N(C4H4), N(C8H6)) and Ph3SnR( R= C6H5) had the pyrrole or not had effect on the character of substituted position. The Mulliken atomic charges of central metal Sn and Ge showed that the atom charge value of Sn and Ge of M(CO)2CY-Ph4X was smaller than M(CO)2CY-Ph3XN (C4H4) and M(CO)2CY-Ph3XN(C8H6) (M=Cr, Mn; X=Sn, Ge; Y=S, Se) correspondingly; electron-donating trend of Ph3GeR group was stronger than that of Ph3SnR group; the pyrrole group had some conjugation effects which made the electronic distribute more even. The calculation results of thermodynamics properties of the synthesize reactions of Ph3SnR(R=N(C4H4), N(C8H6), C6H5) and CpCr(CO)CS showed that the reaction possibility was small at the general condition; ligand CpMn(CO)2CY(Y=S, Se) was more favorable to the reaction than CpCr(CO)2CY(Y=S, Se); different substituted positions would have effect on the reaction possibility apparently. Decreasing temperature would be favorable to the possibility of the reactions, but increasing temperature might be favourable to the rate of reactions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.038
metaresearch head score (Gemma)0.023
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMetaresearch, Meta-epidemiology (narrow), Meta-epidemiology (broad), Bibliometrics, Science and technology studies, Scholarly communication, Open science, Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesMetaresearch, Meta-epidemiology (narrow), Meta-epidemiology (broad), Bibliometrics, Science and technology studies, Scholarly communication, Open science, Research integrity, Insufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.057
Threshold uncertainty score0.996

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0380.023
Meta-epidemiology (narrow)0.0280.030
Meta-epidemiology (broad)0.0280.014
Bibliometrics0.0200.029
Science and technology studies0.0160.016
Scholarly communication0.0110.019
Open science0.0270.015
Research integrity0.0200.022
Insufficient payload (model declined to judge)0.0050.014

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.040
GPT teacher head0.280
Teacher spread0.239 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; both teacher heads agree on what is shown here.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations0
Published2011
Admission routes1
Has abstractyes

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